Crystallography Open Database

Information card for entry 4115943

Preview

Coordinates	4115943.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H21 N Si
Calculated formula	C24 H N Si
Title of publication	Structures of [(Amino)phenylsilyl]lithiums and Related Compounds in Solution and in the Solid State
Authors of publication	Atsushi Kawachi; Kohei Tamao
Journal of publication	Journal of the American Chemical Society
Year of publication	2000
Journal volume	122
Pages of publication	1919 - 1926
a	9.4557 ± 0.0005 Å
b	20.739 ± 0.001 Å
c	10.0569 ± 0.0006 Å
α	90°
β	103.887 ± 0.003°
γ	90°
Cell volume	1914.53 ± 0.18 Å³
Cell temperature	203.2 K
Ambient diffraction temperature	203.2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0617
Residual factor for significantly intense reflections	0.0617
Weighted residual factors for significantly intense reflections	0.0908
Weighted residual factors for all reflections included in the refinement	0.0908
Goodness-of-fit parameter for all reflections included in the refinement	1.151
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4115943.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4115943.cif
70507	2012-12-26	cif/ Adding structures of 4115943 via cif-deposit CGI script.	4115943.cif