Crystallography Open Database

Information card for entry 4115967

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Coordinates	4115967.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H36 Lu N Si3
Calculated formula	C26 H36 Lu N Si3
Title of publication	C2-Symmetric ansa-Lanthanidocene Complexes. Synthesis via Silylamine Elimination and β-SiH Agostic Rigidity
Authors of publication	Jörg Eppinger; Michael Spiegler; Wolfgang Hieringer; Wolfgang A. Herrmann; Reiner Anwander
Journal of publication	Journal of the American Chemical Society
Year of publication	2000
Journal volume	122
Pages of publication	3080 - 3096
a	15.0153 ± 0.0004 Å
b	11.8938 ± 0.0005 Å
c	15.7695 ± 0.0005 Å
α	90°
β	108.145 ± 0.002°
γ	90°
Cell volume	2676.21 ± 0.16 Å³
Cell temperature	273 K
Ambient diffraction temperature	273 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0223
Residual factor for significantly intense reflections	0.0206
Weighted residual factors for significantly intense reflections	0.0469
Weighted residual factors for all reflections included in the refinement	0.0474
Goodness-of-fit parameter for all reflections included in the refinement	1.094
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178930 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/59.	4115967.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4115967.cif
70532	2012-12-27	cif/ Adding structures of 4115967 via cif-deposit CGI script.	4115967.cif