Crystallography Open Database

Information card for entry 4118538

Preview

Coordinates	4118538.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H48 F6 P2 Pt
Calculated formula	C32 H48 F6 P2 Pt
Title of publication	Electrophilic Fluorination of Organoplatinum(II) Iodides: Iodine and Platinum Atoms as Competing Fluorination Sites
Authors of publication	Ina S. Dubinsky-Davidchik; Shay Potash; Israel Goldberg; Arkadi Vigalok; Andrei N. Vedernikov
Journal of publication	Journal of the American Chemical Society
Year of publication	2012
Journal volume	134
Pages of publication	14027 - 14032
a	14.8107 ± 0.0003 Å
b	20.4279 ± 0.0003 Å
c	22.5012 ± 0.0005 Å
α	90°
β	90°
γ	90°
Cell volume	6807.8 ± 0.2 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	5
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.091
Residual factor for significantly intense reflections	0.0507
Weighted residual factors for significantly intense reflections	0.0985
Weighted residual factors for all reflections included in the refinement	0.1099
Goodness-of-fit parameter for all reflections included in the refinement	0.982
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178956 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/85.	4118538.cif
76078	2013-03-15	cif/ Adding structures of 4118538 via cif-deposit CGI script.	4118538.cif