Crystallography Open Database

Information card for entry 4119166

4119165 << 4119166 >> 4119167

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Coordinates	4119166.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H54 Cl N3 O Si6 U
Calculated formula	C18 H54 Cl N3 O Si6 U
Title of publication	Reductive Cleavage of Nitrite to Form Terminal Uranium Mono-Oxo Complexes
Authors of publication	Andrew J. Lewis; Patrick J. Carroll; Eric J. Schelter
Journal of publication	Journal of the American Chemical Society
Year of publication	2013
Journal volume	135
Pages of publication	511 - 518
a	11.8692 ± 0.0004 Å
b	12.5376 ± 0.0004 Å
c	22.9317 ± 0.0008 Å
α	90°
β	90°
γ	90°
Cell volume	3412.5 ± 0.2 Å³
Cell temperature	143 ± 1 K
Ambient diffraction temperature	143 ± 1 K
Number of distinct elements	7
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0216
Residual factor for significantly intense reflections	0.017
Weighted residual factors for significantly intense reflections	0.03
Weighted residual factors for all reflections included in the refinement	0.0307
Goodness-of-fit parameter for all reflections included in the refinement	0.975
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178962 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/91.	4119166.cif
103236	2014-02-27	cif/ Adding structures of 4119166 via cif-deposit CGI script.	4119166.cif