Crystallography Open Database

Information card for entry 4120610

4120609 << 4120610 >> 4120611

Preview

Coordinates	4120610.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C51 H67 N O Si Sn
Calculated formula	C51 H67 N O Si Sn
Title of publication	Low Coordinate Germanium(II) and Tin(II) Hydride Complexes: Efficient Catalysts for the Hydroboration of Carbonyl Compounds.
Authors of publication	Hadlington, Terrance J.; Hermann, Markus; Frenking, Gernot; Jones, Cameron
Journal of publication	Journal of the American Chemical Society
Year of publication	2014
Journal volume	136
Journal issue	8
Pages of publication	3028
a	10.2642 ± 0.0014 Å
b	15.679 ± 0.004 Å
c	28.312 ± 0.004 Å
α	90°
β	98.491 ± 0.013°
γ	90°
Cell volume	4506.4 ± 1.5 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1283
Residual factor for significantly intense reflections	0.059
Weighted residual factors for significantly intense reflections	0.114
Weighted residual factors for all reflections included in the refinement	0.1489
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178983 (current)	2016-03-22	cif/4/12/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/12/06.	4120610.cif
106622	2014-03-15	cif/ Adding structures of 4120610 via cif-deposit CGI script.	4120610.cif