Crystallography Open Database

Information card for entry 4121608

Preview

Coordinates	4121608.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C62 H133 Cl6 Mg4 O12 P2 Pt2 Si2
Calculated formula	C62 H133.162 Cl6 Mg4 O12 P2 Pt2 Si2
Title of publication	1,2-selective hydrosilylation of conjugated dienes.
Authors of publication	Parker, Sarah E.; Börgel, Jonas; Ritter, Tobias
Journal of publication	Journal of the American Chemical Society
Year of publication	2014
Journal volume	136
Journal issue	13
Pages of publication	4857 - 4860
a	8.532 ± 0.0009 Å
b	15.9667 ± 0.0016 Å
c	17.1115 ± 0.0017 Å
α	66.743 ± 0.0016°
β	86.597 ± 0.0018°
γ	82.032 ± 0.0017°
Cell volume	2120.9 ± 0.4 Å³
Cell temperature	100 ± 1 K
Ambient diffraction temperature	100 ± 1 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0379
Residual factor for significantly intense reflections	0.0291
Weighted residual factors for significantly intense reflections	0.0625
Weighted residual factors for all reflections included in the refinement	0.0657
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179018 (current)	2016-03-22	cif/4/12/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/12/16.	4121608.cif
109093	2014-04-08	cif/ Adding structures of 4121608 via cif-deposit CGI script.	4121608.cif