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Information card for entry 4123524
Preview
Coordinates | 4123524.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C18 H24 N2 O7 S |
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Calculated formula | C18 H24 N2 O7 S |
Title of publication | Use of a New Spirophosphine To Achieve Catalytic Enantioselective [4 + 1] Annulations of Amines with Allenes To Generate Dihydropyrroles |
Authors of publication | Kramer, Søren; Fu, Gregory C. |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2015 |
Pages of publication | 150317085953008 |
a | 8.0897 ± 0.0016 Å |
b | 10.667 ± 0.002 Å |
c | 11.916 ± 0.002 Å |
α | 90° |
β | 93.879 ± 0.01° |
γ | 90° |
Cell volume | 1025.9 ± 0.3 Å3 |
Cell temperature | 293 K |
Ambient diffraction temperature | 293 K |
Number of distinct elements | 5 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.067 |
Residual factor for significantly intense reflections | 0.0411 |
Weighted residual factors for significantly intense reflections | 0.1057 |
Weighted residual factors for all reflections included in the refinement | 0.1168 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.923 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
179037 (current) | 2016-03-22 | cif/4/12/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/12/35. |
4123524.cif |
133998 | 2015-03-18 | cif/ Adding structures of 4123521, 4123522, 4123523, 4123524 via cif-deposit CGI script. |
4123524.cif |
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Users of the data should acknowledge the original authors of the
structural data.