Crystallography Open Database

Information card for entry 4123565

Preview

Coordinates	4123565.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	{(cAAC)Si(P-Tip)}2
Formula	C172 H271 N4 P4 Si4
Calculated formula	C172 H271 N4 P4 Si4
Title of publication	Carbene supported dimer of heavier ketenimine analogue with p and si atoms.
Authors of publication	Roy, Sudipta; Dittrich, Birger; Mondal, Totan; Koley, Debasis; Stückl, A Claudia; Schwederski, Brigitte; Kaim, Wolfgang; John, Michael; Vasa, Suresh Kumar; Linser, Rasmus; Roesky, Herbert W.
Journal of publication	Journal of the American Chemical Society
Year of publication	2015
Journal volume	137
Journal issue	19
Pages of publication	6180 - 6183
a	15.5998 ± 0.0006 Å
b	10.9274 ± 0.0005 Å
c	46.7138 ± 0.0019 Å
α	90°
β	93.599 ± 0.003°
γ	90°
Cell volume	7947.4 ± 0.6 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0778
Residual factor for significantly intense reflections	0.0495
Weighted residual factors for significantly intense reflections	0.0986
Weighted residual factors for all reflections included in the refinement	0.1097
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
138242 (current)	2015-06-05	cif/ Updating files of 4123565 Original log message: Adding full bibliography for 4123565.cif.	4123565.cif
136265	2015-05-13	cif/ Adding structures of 4123565 via cif-deposit CGI script.	4123565.cif