Crystallography Open Database

Information card for entry 4124459

Preview

Coordinates	4124459.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C76 H75 B F24 Ge N2 O3 Si W
Calculated formula	C76 H75 B F24 Ge N2 O3 Si W
Title of publication	Insertion of a Cationic Metallogermylene into E-H Bonds (E = H, B, Si).
Authors of publication	Inomata, Koya; Watanabe, Takahito; Miyazaki, Yoshikazu; Tobita, Hiromi
Journal of publication	Journal of the American Chemical Society
Year of publication	2015
Journal volume	137
Journal issue	37
Pages of publication	11935 - 11937
a	16.2451 ± 0.0005 Å
b	22.0047 ± 0.0009 Å
c	25.4722 ± 0.001 Å
α	64.8116 ± 0.001°
β	77.7275 ± 0.0007°
γ	76.6013 ± 0.0007°
Cell volume	7948 ± 0.5 Å³
Cell temperature	140 ± 2 K
Ambient diffraction temperature	140 ± 2 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1049
Residual factor for significantly intense reflections	0.0732
Weighted residual factors for significantly intense reflections	0.1629
Weighted residual factors for all reflections included in the refinement	0.1798
Goodness-of-fit parameter for all reflections included in the refinement	1.117
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	4124459.cif
160539	2015-10-06	cif/ Updating files of 4124458, 4124459 Original log message: Adding full bibliography for 4124458--4124459.cif.	4124459.cif
155830	2015-09-10	cif/ Adding structures of 4124458, 4124459 via cif-deposit CGI script.	4124459.cif