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Information card for entry 4125696
Preview
| Coordinates | 4125696.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C67 H73 Cl4 N3 O3 Os P2 |
|---|---|
| Calculated formula | C67 H67 Cl4 N3 O3 Os P2 |
| Title of publication | Reactions of Isocyanides with Metal Carbyne Complexes: Isolation and Characterization of Metallacyclopropenimine Intermediates. |
| Authors of publication | Luo, Ming; Long, Lipeng; Zhang, Hong; Yang, Yuhui; Hua, Yuhui; Liu, Gang; Lin, Zhenyang; Xia, Haiping |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2017 |
| Journal volume | 139 |
| Journal issue | 5 |
| Pages of publication | 1822 - 1825 |
| a | 11.6666 ± 0.0004 Å |
| b | 12.6271 ± 0.0004 Å |
| c | 22.2623 ± 0.0006 Å |
| α | 93.498 ± 0.002° |
| β | 98.272 ± 0.002° |
| γ | 108.058 ± 0.003° |
| Cell volume | 3066.1 ± 0.18 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.047 |
| Residual factor for significantly intense reflections | 0.0392 |
| Weighted residual factors for significantly intense reflections | 0.0906 |
| Weighted residual factors for all reflections included in the refinement | 0.0936 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.053 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 193090 (current) | 2017-03-04 | cif/ Adding structures of 4125693, 4125694, 4125695, 4125696 via cif-deposit CGI script. |
4125696.cif |
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Users of the data should acknowledge the original authors of the
structural data.