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Information card for entry 4125721
Preview
| Coordinates | 4125721.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C22 H37 B O3 Si |
|---|---|
| Calculated formula | C22 H37 B O3 Si |
| Title of publication | Diastereoselective Borocyclopropanation of Allylic Ethers Using a Boromethylzinc Carbenoid. |
| Authors of publication | Benoit, Guillaume; Charette, André B |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2017 |
| Journal volume | 139 |
| Journal issue | 4 |
| Pages of publication | 1364 - 1367 |
| a | 6.6124 ± 0.0003 Å |
| b | 11.5841 ± 0.0005 Å |
| c | 30.0883 ± 0.0011 Å |
| α | 90° |
| β | 92.3994 ± 0.0018° |
| γ | 90° |
| Cell volume | 2302.7 ± 0.17 Å3 |
| Cell temperature | 100 K |
| Ambient diffraction temperature | 100 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0769 |
| Residual factor for significantly intense reflections | 0.0702 |
| Weighted residual factors for significantly intense reflections | 0.1892 |
| Weighted residual factors for all reflections included in the refinement | 0.1948 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.063 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 193100 (current) | 2017-03-04 | cif/ Adding structures of 4125721 via cif-deposit CGI script. |
4125721.cif |
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Users of the data should acknowledge the original authors of the
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