Crystallography Open Database

Information card for entry 4130346

Preview

Coordinates	4130346.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C384 H264 F144 Fe8 N48 O24 P16
Calculated formula	C384 H264 F96 Fe8 N48 O24 P8
Title of publication	Perfluorinated Ligands Induce Meridional Metal Stereochemistry to Generate M8L12, M10L15, and M12L18 Prisms.
Authors of publication	Kieffer, Marion; Pilgrim, Ben S.; Ronson, Tanya K.; Roberts, Derrick A.; Aleksanyan, Mina; Nitschke, Jonathan R.
Journal of publication	Journal of the American Chemical Society
Year of publication	2016
Journal volume	138
Journal issue	21
Pages of publication	6813 - 6821
a	38.41 ± 0.006 Å
b	38.41 ± 0.006 Å
c	38.41 ± 0.006 Å
α	90°
β	90°
γ	90°
Cell volume	56667 ± 15 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	207
Hermann-Mauguin space group symbol	P 4 3 2
Hall space group symbol	P 4 2 3
Residual factor for all reflections	0.2193
Residual factor for significantly intense reflections	0.2083
Weighted residual factors for significantly intense reflections	0.4624
Weighted residual factors for all reflections included in the refinement	0.4721
Goodness-of-fit parameter for all reflections included in the refinement	1.541
Diffraction radiation wavelength	0.6889 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
240809 (current)	2019-11-25	cif/ Adding structures of 4130345, 4130346 via cif-deposit CGI script.	4130346.cif