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Information card for entry 4131299
Preview
| Coordinates | 4131299.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C36 H46 Hf O Si3 |
|---|---|
| Calculated formula | C36 H46 Hf O Si3 |
| Title of publication | A Stable Silylene with a σ<sup>2</sup>, π- Butadiene Ligand. |
| Authors of publication | Dong, Zhaowen; Reinhold, Crispin R. W.; Schmidtmann, Marc; Müller, Thomas |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2017 |
| Journal volume | 139 |
| Journal issue | 20 |
| Pages of publication | 7117 - 7123 |
| a | 39.33 ± 0.003 Å |
| b | 7.9638 ± 0.0006 Å |
| c | 10.8208 ± 0.0008 Å |
| α | 90° |
| β | 93.2487 ± 0.0015° |
| γ | 90° |
| Cell volume | 3383.8 ± 0.4 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 5 |
| Hermann-Mauguin space group symbol | C 1 2 1 |
| Hall space group symbol | C 2y |
| Residual factor for all reflections | 0.0274 |
| Residual factor for significantly intense reflections | 0.0246 |
| Weighted residual factors for significantly intense reflections | 0.0505 |
| Weighted residual factors for all reflections included in the refinement | 0.0512 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.095 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 241531 (current) | 2019-11-25 | cif/ Adding structures of 4131299 via cif-deposit CGI script. |
4131299.cif |
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Users of the data should acknowledge the original authors of the
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