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Information card for entry 4131797
Preview
| Coordinates | 4131797.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C107 H170 Al2 Ir2 N4 Si4 |
|---|---|
| Calculated formula | C107 H170 Al2 Ir2 N4 Si4 |
| Title of publication | Aluminabenzene-Rh and -Ir Complexes: Synthesis, Structure, and Application toward Catalytic C-H Borylation. |
| Authors of publication | Nakamura, Taichi; Suzuki, Katsunori; Yamashita, Makoto |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2017 |
| Journal volume | 139 |
| Journal issue | 49 |
| Pages of publication | 17763 - 17766 |
| a | 13.4845 ± 0.0016 Å |
| b | 14.673 ± 0.0016 Å |
| c | 14.8811 ± 0.0019 Å |
| α | 73.347 ± 0.007° |
| β | 71.377 ± 0.007° |
| γ | 68.568 ± 0.007° |
| Cell volume | 2548.6 ± 0.5 Å3 |
| Cell temperature | 93 ± 2 K |
| Ambient diffraction temperature | 93 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0747 |
| Residual factor for significantly intense reflections | 0.0602 |
| Weighted residual factors for significantly intense reflections | 0.117 |
| Weighted residual factors for all reflections included in the refinement | 0.1257 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.068 |
| Diffraction radiation wavelength | 0.71075 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 241946 (current) | 2019-11-25 | cif/ Adding structures of 4131794, 4131795, 4131796, 4131797 via cif-deposit CGI script. |
4131797.cif |
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Users of the data should acknowledge the original authors of the
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