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Information card for entry 4132230
Preview
| Coordinates | 4132230.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C39 H56 As Ga N2 |
|---|---|
| Calculated formula | C39 H56 As Ga N2 |
| Title of publication | Synthesis of a Gallaarsene {HC[C(Me)N-2,6- i-Pr<sub>2</sub>-C<sub>6</sub>H<sub>3</sub>]<sub>2</sub>}GaAsCp* Containing a Ga═As Double Bond. |
| Authors of publication | Helling, Christoph; Wölper, Christoph; Schulz, Stephan |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2018 |
| Journal volume | 140 |
| Journal issue | 15 |
| Pages of publication | 5053 - 5056 |
| a | 11.8364 ± 0.0005 Å |
| b | 18.1069 ± 0.0008 Å |
| c | 18.3359 ± 0.0008 Å |
| α | 87.481 ± 0.002° |
| β | 81.731 ± 0.002° |
| γ | 73.919 ± 0.002° |
| Cell volume | 3736.7 ± 0.3 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0473 |
| Residual factor for significantly intense reflections | 0.0324 |
| Weighted residual factors for significantly intense reflections | 0.0754 |
| Weighted residual factors for all reflections included in the refinement | 0.0822 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.028 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 242231 (current) | 2019-11-26 | cif/ Adding structures of 4132229, 4132230 via cif-deposit CGI script. |
4132230.cif |
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Users of the data should acknowledge the original authors of the
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