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Information card for entry 4132238
Preview
| Coordinates | 4132238.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C32 H30 O14.05 |
|---|---|
| Calculated formula | C32 H30 O14.049 |
| Title of publication | Asymmetric Synthesis of Gonytolide A: Strategic Use of an Aryl Halide Blocking Group for Oxidative Coupling. |
| Authors of publication | Wu, Xiaowei; Iwata, Takayuki; Scharf, Adam; Qin, Tian; Reichl, Kyle D.; Porco, Jr, John A |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2018 |
| Journal volume | 140 |
| Journal issue | 18 |
| Pages of publication | 5969 - 5975 |
| a | 12.8266 ± 0.0006 Å |
| b | 13.9034 ± 0.0007 Å |
| c | 16.8142 ± 0.0008 Å |
| α | 90° |
| β | 101.097 ± 0.002° |
| γ | 90° |
| Cell volume | 2942.5 ± 0.2 Å3 |
| Cell temperature | 100 K |
| Ambient diffraction temperature | 99.89 K |
| Number of distinct elements | 3 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0372 |
| Residual factor for significantly intense reflections | 0.0361 |
| Weighted residual factors for significantly intense reflections | 0.0957 |
| Weighted residual factors for all reflections included in the refinement | 0.0967 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.027 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 242239 (current) | 2019-11-26 | cif/ Adding structures of 4132238 via cif-deposit CGI script. |
4132238.cif |
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Users of the data should acknowledge the original authors of the
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