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Information card for entry 4132373
Preview
| Coordinates | 4132373.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H52 B Cl Li2 O2 Si4 |
|---|---|
| Calculated formula | C24 H52 B Cl Li2 O2 Si4 |
| Title of publication | From Borapyramidane to Borole Dianion. |
| Authors of publication | Lee, Vladimir Ya; Sugasawa, Haruka; Gapurenko, Olga A.; Minyaev, Ruslan M.; Minkin, Vladimir I.; Gornitzka, Heinz; Sekiguchi, Akira |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2018 |
| Journal volume | 140 |
| Journal issue | 19 |
| Pages of publication | 6053 - 6056 |
| a | 9.2197 ± 0.0015 Å |
| b | 20.178 ± 0.003 Å |
| c | 18.246 ± 0.003 Å |
| α | 90° |
| β | 103.57 ± 0.002° |
| γ | 90° |
| Cell volume | 3299.6 ± 0.9 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0693 |
| Residual factor for significantly intense reflections | 0.0509 |
| Weighted residual factors for significantly intense reflections | 0.1173 |
| Weighted residual factors for all reflections included in the refinement | 0.1259 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.073 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 242356 (current) | 2019-11-26 | cif/ Adding structures of 4132373 via cif-deposit CGI script. |
4132373.cif |
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