Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4132864
Preview
| Coordinates | 4132864.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C165 H252 Li8 N8 |
|---|---|
| Calculated formula | C165 H252 Li8 N8 |
| Title of publication | New Hindered Amide Base for Aryne Insertion into Si-P, Si-S, Si-N, and C-C Bonds. |
| Authors of publication | Mesgar, Milad; Nguyen-Le, Justin; Daugulis, Olafs |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2018 |
| Journal volume | 140 |
| Journal issue | 42 |
| Pages of publication | 13703 - 13710 |
| a | 11.8908 ± 0.0003 Å |
| b | 15.5218 ± 0.0003 Å |
| c | 19.7689 ± 0.0005 Å |
| α | 95.344 ± 0.001° |
| β | 90.555 ± 0.001° |
| γ | 108.045 ± 0.001° |
| Cell volume | 3451.27 ± 0.14 Å3 |
| Cell temperature | 123 ± 2 K |
| Ambient diffraction temperature | 123 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0668 |
| Residual factor for significantly intense reflections | 0.0591 |
| Weighted residual factors for significantly intense reflections | 0.1575 |
| Weighted residual factors for all reflections included in the refinement | 0.1674 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.014 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 242752 (current) | 2019-11-26 | cif/ Adding structures of 4132864 via cif-deposit CGI script. |
4132864.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.