Crystallography Open Database

Information card for entry 4133532

Preview

Coordinates	4133532.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H66.5 N8 O35 S6 V5 W
Calculated formula	C14 H54.5 N7 O39 S7 V5 W
Title of publication	Self-Assembly of Goldberg Polyhedra from a Concave [WV<sub>5</sub>O<sub>11</sub>(RCO<sub>2</sub>)<sub>5</sub>(SO<sub>4</sub>)]<sup>3-</sup> Building Block with 5-Fold Symmetry.
Authors of publication	Zhang, Yuteng; Gan, Hongmei; Qin, Chao; Wang, Xinlong; Su, Zhongmin; Zaworotko, Michael J.
Journal of publication	Journal of the American Chemical Society
Year of publication	2018
Journal volume	140
Journal issue	50
Pages of publication	17365 - 17368
a	15.49 ± 0.005 Å
b	16.481 ± 0.005 Å
c	21.309 ± 0.005 Å
α	90°
β	90°
γ	90°
Cell volume	5440 ± 3 Å³
Cell temperature	296 K
Ambient diffraction temperature	296 K
Number of distinct elements	7
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0405
Residual factor for significantly intense reflections	0.0379
Weighted residual factors for significantly intense reflections	0.102
Weighted residual factors for all reflections included in the refinement	0.1037
Goodness-of-fit parameter for all reflections included in the refinement	1.122
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
243297 (current)	2019-11-26	cif/ Adding structures of 4133532, 4133533, 4133534, 4133535, 4133536, 4133537 via cif-deposit CGI script.	4133532.cif