Crystallography Open Database

Information card for entry 4135384

Preview

Coordinates	4135384.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C51 H76 Al2 N4 O4 P4 Rh2
Calculated formula	C51 H76 Al2 N4 O4 P4 Rh2
Title of publication	Unexpected B/Al Transelementation within a Rh Pincer Complex.
Authors of publication	Lai, Qingheng; Bhuvanesh, Nattamai; Ozerov, Oleg V.
Journal of publication	Journal of the American Chemical Society
Year of publication	2020
Journal volume	142
Journal issue	50
Pages of publication	20920 - 20923
a	15.278 ± 0.0005 Å
b	9.6009 ± 0.0003 Å
c	19.5396 ± 0.0006 Å
α	90°
β	93.389 ± 0.002°
γ	90°
Cell volume	2861.11 ± 0.16 Å³
Cell temperature	110 K
Ambient diffraction temperature	110 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0272
Residual factor for significantly intense reflections	0.0213
Weighted residual factors for significantly intense reflections	0.0483
Weighted residual factors for all reflections included in the refinement	0.0509
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
260429 (current)	2021-01-04	cif/ Updating files of 4135382, 4135383, 4135384 Original log message: Adding full bibliography for 4135382--4135384.cif.	4135384.cif
259471	2020-12-03	cif/ Adding structures of 4135382, 4135383, 4135384 via cif-deposit CGI script.	4135384.cif