Crystallography Open Database

Information card for entry 4135393

Preview

Coordinates	4135393.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C131 H141 Cl4 F3 N12 P8 Pd4
Calculated formula	C131 H141 Cl4 F3 N12 P8 Pd4
Title of publication	Enthalpy-Controlled Insertion of a "Nonspectator" Tricoordinate Phosphorus Ligand into Group 10 Transition Metal-Carbon Bonds.
Authors of publication	Hwang, Seung Jun; Tanushi, Akira; Radosevich, Alexander T.
Journal of publication	Journal of the American Chemical Society
Year of publication	2020
Journal volume	142
Journal issue	51
Pages of publication	21285 - 21291
a	15.426 ± 0.003 Å
b	15.426 ± 0.003 Å
c	26.835 ± 0.006 Å
α	90°
β	90°
γ	90°
Cell volume	6386 ± 2 Å³
Cell temperature	15 ± 2 K
Ambient diffraction temperature	15 K
Number of distinct elements	7
Space group number	114
Hermann-Mauguin space group symbol	P -4 21 c
Hall space group symbol	P -4 2n
Residual factor for all reflections	0.0425
Residual factor for significantly intense reflections	0.0371
Weighted residual factors for significantly intense reflections	0.097
Weighted residual factors for all reflections included in the refinement	0.1018
Goodness-of-fit parameter for all reflections included in the refinement	1.087
Diffraction radiation wavelength	0.24797 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
260425 (current)	2021-01-04	cif/ Updating files of 4135390, 4135391, 4135392, 4135393 Original log message: Adding full bibliography for 4135390--4135393.cif.	4135393.cif
259846	2020-12-13	cif/ Adding structures of 4135393 via cif-deposit CGI script.	4135393.cif