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Information card for entry 4303342
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| Coordinates | 4303342.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | sodium 15-crown-5 trisulfur trintride |
|---|---|
| Formula | C10 H20 N3 Na O5 S3 |
| Calculated formula | C10 H20 N3 Na O5 S3 |
| Title of publication | Electrochemical and Chemical Reduction of Disulfur Dinitride: Formation of [S4N4]-., EPR Spectroscopic Characterization of the [S2N2H]. Radical, and X-ray Structure of [Na(15-crown-5)][S3N3] |
| Authors of publication | Tracey L. Roemmele; Jari Konu; René T. Boeré; Tristram Chivers |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2009 |
| Journal volume | 48 |
| Pages of publication | 9454 - 9462 |
| a | 16.158 ± 0.003 Å |
| b | 14.383 ± 0.003 Å |
| c | 7.3713 ± 0.0015 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 1713.1 ± 0.6 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 62 |
| Hermann-Mauguin space group symbol | P n m a |
| Hall space group symbol | -P 2ac 2n |
| Residual factor for all reflections | 0.0952 |
| Residual factor for significantly intense reflections | 0.0546 |
| Weighted residual factors for significantly intense reflections | 0.1267 |
| Weighted residual factors for all reflections included in the refinement | 0.1479 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.032 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 192779 (current) | 2017-03-02 | cif/4/30/33/ (antanas@echidna.ibt.lt) Replacing data items '_publ_contact_author1', '_publ_contact_author2', '_publ_contact_author1_email' and '_publ_contact_author2_email' with the _publ_contact_author* loop in entry 4303342. |
4303342.cif |
| 179071 | 2016-03-22 | cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/33. |
4303342.cif |
| 120081 | 2014-07-12 | Adding DOIs to range 4/30 structures. | 4303342.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4303342.cif |
| 1125 | 2010-04-25 | cif/4/ Adding CIFs for the Inorg-Chem-2009_11-24 deposition. |
4303342.cif |
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