Crystallography Open Database

Information card for entry 4303789

Preview

Coordinates	4303789.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Ga4 H14 N3 O2 S9 Sb
Calculated formula	Ga4 N3 O2 S9 Sb
Title of publication	Three-Dimensional Frameworks of Cubic (NH4)5Ga4SbS10, (NH4)4Ga4SbS9(OH).H2O, and (NH4)3Ga4SbS9(OH2).2H2O
Authors of publication	Joshua L. Mertz; Nan Ding; Mercouri G. Kanatzidis
Journal of publication	Inorganic Chemistry
Year of publication	2009
Journal volume	48
Pages of publication	10898 - 10900
a	12.9045 ± 0.0006 Å
b	12.9045 ± 0.0006 Å
c	12.9045 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	2148.94 ± 0.17 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	6
Space group number	198
Hermann-Mauguin space group symbol	P 21 3
Hall space group symbol	P 2ac 2ab 3
Residual factor for all reflections	0.0459
Residual factor for significantly intense reflections	0.0393
Weighted residual factors for significantly intense reflections	0.1167
Weighted residual factors for all reflections included in the refinement	0.1239
Goodness-of-fit parameter for all reflections included in the refinement	0.957
Diffraction radiation wavelength	0.41328 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179075 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/37.	4303789.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4303789.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4303789.cif
1125	2010-04-25	cif/4/ Adding CIFs for the Inorg-Chem-2009_11-24 deposition.	4303789.cif