Crystallography Open Database

Information card for entry 4303974

Preview

Coordinates	4303974.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H50 Co Mo12 N12 O50
Calculated formula	C18 H30 Co Mo12 N12 O50
Title of publication	Cobalt(II)/Nickel(II)-Centered Keggin-Type Heteropolymolybdates: Syntheses, Crystal Structures, Magnetic and Electrochemical Properties
Authors of publication	Guang-Gang Gao; Lin Xu; Wen-Ju Wang; Xiao-Shu Qu; Hong Liu; Yan-Yan Yang
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	2325 - 2333
a	13.043 ± 0.002 Å
b	21.364 ± 0.003 Å
c	21.676 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	6040 ± 1.5 Å³
Cell temperature	185 ± 2 K
Ambient diffraction temperature	185 ± 2 K
Number of distinct elements	6
Space group number	69
Hermann-Mauguin space group symbol	F m m m
Hall space group symbol	-F 2 2
Residual factor for all reflections	0.1114
Residual factor for significantly intense reflections	0.059
Weighted residual factors for significantly intense reflections	0.1264
Weighted residual factors for all reflections included in the refinement	0.144
Goodness-of-fit parameter for all reflections included in the refinement	0.957
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179077 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/39.	4303974.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4303974.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4303974.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4303974.cif