Crystallography Open Database

Information card for entry 4303990

Preview

Coordinates	4303990.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C75 H112 P4 Sn2
Calculated formula	C75 H104 P4 Sn2
Title of publication	Unusual Reactivity of Methylphosphaalkyne (P\τbCMe) toward Digermenes and Distannenes: Stepwise Formations of Bridged 2,3,5,6-Tetraphospha-1,4-dimethylidenecyclohexanes
Authors of publication	Cameron Jones; Christian Schulten; Andreas Stasch
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	1273 - 1278
a	10.727 ± 0.002 Å
b	12.633 ± 0.003 Å
c	14.198 ± 0.003 Å
α	71.7 ± 0.03°
β	80.66 ± 0.03°
γ	83.61 ± 0.03°
Cell volume	1798.8 ± 0.7 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0361
Residual factor for significantly intense reflections	0.0312
Weighted residual factors for significantly intense reflections	0.0698
Weighted residual factors for all reflections included in the refinement	0.0723
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179077 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/39.	4303990.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4303990.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4303990.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4303990.cif