Crystallography Open Database

Information card for entry 4304210

Preview

Coordinates	4304210.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H66 N3 Pu Si6
Calculated formula	C18 H54 N3 Pu Si6
Title of publication	Structural Characterization of Pu[N(SiMe3)2]3, a Synthetically Useful Nonaqueous Plutonium(III) Precursor
Authors of publication	Andrew J. Gaunt; Alejandro E. Enriquez; Sean D. Reilly; Brian L. Scott; Mary P. Neu
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	26 - 28
a	16.404 ± 0.005 Å
b	16.404 ± 0.005 Å
c	8.306 ± 0.005 Å
α	90°
β	90°
γ	120°
Cell volume	1935.6 ± 1.4 Å³
Cell temperature	141 ± 2 K
Ambient diffraction temperature	141 ± 2 K
Number of distinct elements	5
Space group number	163
Hermann-Mauguin space group symbol	P -3 1 c
Hall space group symbol	-P 3 2c
Residual factor for all reflections	0.1026
Residual factor for significantly intense reflections	0.0705
Weighted residual factors for significantly intense reflections	0.1628
Weighted residual factors for all reflections included in the refinement	0.1787
Goodness-of-fit parameter for all reflections included in the refinement	1.102
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179080 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/42.	4304210.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4304210.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4304210.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4304210.cif