Crystallography Open Database

Information card for entry 4304237

Preview

Coordinates	4304237.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C832 H992 K48 N48 O88
Calculated formula	C832 H992 K48 N48 O88
Title of publication	Potassium Hydroxylamine Complexes
Authors of publication	Ajay Venugopal; Raphael J. F. Berger; Alexander Willner; Tania Pape; Norbert W. Mitzel
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	4506 - 4512
a	56.511 ± 0.006 Å
b	14.5171 ± 0.0015 Å
c	26.289 ± 0.003 Å
α	90°
β	112.013 ± 0.002°
γ	90°
Cell volume	19995 ± 4 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1646
Residual factor for significantly intense reflections	0.0795
Weighted residual factors for significantly intense reflections	0.1583
Weighted residual factors for all reflections included in the refinement	0.1907
Goodness-of-fit parameter for all reflections included in the refinement	1.012
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179080 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/42.	4304237.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4304237.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4304237.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4304237.cif