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Information card for entry 4304396
Preview
| Coordinates | 4304396.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C35 H36 Cl4 N4 Os P2 |
|---|---|
| Calculated formula | C35 H36 Cl4 N4 Os P2 |
| SMILES | [Os]12(Cl)([P](CC[n]3n1ccc3)(c1ccccc1)c1ccccc1)(Cl)[P](CC[n]1n2ccc1)(c1ccccc1)c1ccccc1.ClCCl |
| Title of publication | Ru and Os Complexes Containing a P,N-Donor Heterotopic Ligand: The Effect of Solvent on Stereochemistry |
| Authors of publication | Dabb, Serin L.; Messerle, Barbara A.; Smith, Matthew K.; Willis, Anthony C. |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2008 |
| Journal volume | 47 |
| Journal issue | 8 |
| Pages of publication | 3034 - 3044 |
| a | 10.25 ± 0.002 Å |
| b | 19.019 ± 0.004 Å |
| c | 37.938 ± 0.008 Å |
| α | 90° |
| β | 92.48 ± 0.03° |
| γ | 90° |
| Cell volume | 7389 ± 3 Å3 |
| Cell temperature | 200 ± 2 K |
| Ambient diffraction temperature | 200 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.1025 |
| Residual factor for significantly intense reflections | 0.0679 |
| Weighted residual factors for significantly intense reflections | 0.1156 |
| Weighted residual factors for all reflections included in the refinement | 0.1254 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.23 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 210348 (current) | 2018-09-02 | cif/4/ Updating bibliography in entries 4304395-4304400, 4333500. Marking entry 4333500 as a duplicate of entry 4304396, |
4304396.cif |
| 179081 | 2016-03-22 | cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/43. |
4304396.cif |
| 120081 | 2014-07-12 | Adding DOIs to range 4/30 structures. | 4304396.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4304396.cif |
| 32063 | 2012-01-26 | cif/4 Correction of volume and publication year for files coming from a couple of issues of Inorg. Chem. The mistake was made when fetching bibliography for these entries and detected just now. I have checked that all other Inorg. Chem. files are correct. |
4304396.cif |
| 1163 | 2010-05-11 | cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition. | 4304396.cif |
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