Crystallography Open Database

Information card for entry 4304420

Preview

Coordinates	4304420.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H22 Cl2 N O0.5 Re
Calculated formula	C19 H22 Cl2 N O0.5 Re
Title of publication	Oxygen-Centered Hexatantalum Tetradecaimido Cluster Complexes
Authors of publication	Jamin L. Krinsky; Laura L. Anderson; John Arnold; Robert G. Bergman
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	1053 - 1066
a	8.4832 ± 0.0015 Å
b	17.131 ± 0.003 Å
c	13.904 ± 0.002 Å
α	90°
β	102.723 ± 0.002°
γ	90°
Cell volume	1971 ± 0.6 Å³
Cell temperature	157 ± 2 K
Ambient diffraction temperature	157 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0403
Residual factor for significantly intense reflections	0.0256
Weighted residual factors for significantly intense reflections	0.0544
Weighted residual factors for all reflections included in the refinement	0.0575
Goodness-of-fit parameter for all reflections included in the refinement	1.114
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4304420.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4304420.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4304420.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4304420.cif