Crystallography Open Database

Information card for entry 4304433

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Coordinates	4304433.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Tetrabutyammonium tris(μ~2~-chloro)-bis(trichloro-platinum(iv))
Formula	C16 H36 Cl9 N Pt2
Calculated formula	C16 H36 Cl9 N Pt2
Title of publication	Simple Preparations of Pd6Cl12, Pt6Cl12, and Qn[Pt2Cl8+n], n= 1, 2 (Q = TBA+, PPN+) and Structural Characterization of [TBA][Pt2Cl9] and [PPN]2[Pt2Cl10].C7H8
Authors of publication	Daniela Belli Dell'Amico; Fausto Calderazzo; Fabio Marchetti; Stefano Ramello; Simona Samaritani
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	1237 - 1242
a	10.637 ± 0.002 Å
b	11.1555 ± 0.0019 Å
c	14.006 ± 0.002 Å
α	90°
β	111.86 ± 0.013°
γ	90°
Cell volume	1542.5 ± 0.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.1217
Residual factor for significantly intense reflections	0.0654
Weighted residual factors for significantly intense reflections	0.1567
Weighted residual factors for all reflections included in the refinement	0.1881
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179082 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/44.	4304433.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4304433.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4304433.cif
5312	2011-01-03	cif/ Adding files, updated with the 'cif_fix_enum' program and the cif_core.dic dictionary. The enumerator values were fixed, mostly incorrect case, but also some values that had extra underscores, dashes or spaces. Unfortunately, 22 had non-ASCII characters with the 8-th bit set, and these got incorrectly interpreted as latin1 characters and converted to their UTF8 equivalents by Perl. To fix the structures, however, they need to be redeposited from the original files with the new CIFParser/cif_filter version.	4304433.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4304433.cif