Crystallography Open Database

Information card for entry 4304517

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Coordinates	4304517.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	catena-[bis(?4-succinato)-bis(?2-chloro) -di-manganese(ii)]-bis(ethylenediamine)-copper(ii)
Formula	C12 H24 Cl2 Cu Mn2 N4 O8
Calculated formula	C12 H24 Cl2 Cu Mn2 N4 O8
Title of publication	Direct Synthesis, Crystal Structures, High-Field EPR, and Magnetic Studies of Heterometallic Polymers Containing Manganese(II) Carboxylates Interconnected by [Cu(en)2]2+
Authors of publication	Valeriya G. Makhankova; Asya O. Beznischenko; Vladimir N. Kokozay; Roman I. Zubatyuk; Oleg V. Shishkin; Julia Jezierska; Andrew Ozarowski
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	4554 - 4563
a	6.5384 ± 0.0004 Å
b	8.3059 ± 0.0007 Å
c	10.962 ± 0.0006 Å
α	110.646 ± 0.007°
β	94.732 ± 0.005°
γ	106.16 ± 0.006°
Cell volume	524.16 ± 0.07 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.037
Residual factor for significantly intense reflections	0.0333
Weighted residual factors for significantly intense reflections	0.0875
Weighted residual factors for all reflections included in the refinement	0.0908
Goodness-of-fit parameter for all reflections included in the refinement	1.155
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179083 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/45.	4304517.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4304517.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4304517.cif
5312	2011-01-03	cif/ Adding files, updated with the 'cif_fix_enum' program and the cif_core.dic dictionary. The enumerator values were fixed, mostly incorrect case, but also some values that had extra underscores, dashes or spaces. Unfortunately, 22 had non-ASCII characters with the 8-th bit set, and these got incorrectly interpreted as latin1 characters and converted to their UTF8 equivalents by Perl. To fix the structures, however, they need to be redeposited from the original files with the new CIFParser/cif_filter version.	4304517.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4304517.cif