Crystallography Open Database

Information card for entry 4304837

Preview

Coordinates	4304837.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C70 H98 Mo2 O12 P2 Sn2
Calculated formula	C70 H98 Mo2 O12 P2 Sn2
Title of publication	From Coordinated Oxophosphinidene to O,O,P-Bound Arylhypophosphite(2-) To Build a Singular Mo2Sn2O4P2 Metallocycle
Authors of publication	María Alonso; M. Angeles Alvarez; M. Esther García; Miguel A. Ruiz
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	1252 - 1254
a	19.449 ± 0.007 Å
b	14.367 ± 0.005 Å
c	27.4 ± 0.01 Å
α	90°
β	101.748 ± 0.006°
γ	90°
Cell volume	7496 ± 5 Å³
Cell temperature	120 ± 0.1 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0806
Residual factor for significantly intense reflections	0.0499
Weighted residual factors for significantly intense reflections	0.1171
Weighted residual factors for all reflections included in the refinement	0.1273
Goodness-of-fit parameter for all reflections included in the refinement	1.02
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179086 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/48.	4304837.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4304837.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4304837.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4304837.cif