Crystallography Open Database

Information card for entry 4304899

Preview

Coordinates	4304899.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C68 H136 Cl8 La2 N12 O27
Calculated formula	C67.99 H132 Cl8 La2 N12 O27
Title of publication	Lanthanum(III) and Uranyl(VI) Diglycolamide Complexes: Synthetic Precursors and Structural Studies Involving Nitrate Complexation
Authors of publication	Shanmugaperumal Kannan; Morgan A. Moody; Charles L. Barnes; Paul B. Duval
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	4691 - 4695
a	14.4936 ± 0.0003 Å
b	14.4936 ± 0.0003 Å
c	82.795 ± 0.003 Å
α	90°
β	90°
γ	120°
Cell volume	15062.2 ± 0.7 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	161
Hermann-Mauguin space group symbol	R 3 c :H
Hall space group symbol	R 3 -2"c
Residual factor for all reflections	0.0583
Residual factor for significantly intense reflections	0.0373
Weighted residual factors for significantly intense reflections	0.0871
Weighted residual factors for all reflections included in the refinement	0.0948
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179086 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/48.	4304899.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4304899.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4304899.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4304899.cif