Crystallography Open Database

Information card for entry 4306611

Preview

Coordinates	4306611.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Gd(^i^PrN)~2~CNMe~2~ (1b)
Formula	C27 H60 Gd N9
Calculated formula	C27 H60 Gd N9
SMILES	[Gd]123([N](C(C)C)=C(N1C(C)C)N(C)C)([N](=C(N2C(C)C)N(C)C)C(C)C)[N](=C(N3C(C)C)N(C)C)C(C)C
Title of publication	Synthesis, Characterization, and Thermal Properties of Homoleptic Rare-Earth Guanidinates: Promising Precursors for MOCVD and ALD of Rare-Earth Oxide Thin Films
Authors of publication	Andrian P. Milanov; Roland A. Fischer; Anjana Devi
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	11405 - 11416
a	10.7314 ± 0.0002 Å
b	11.2394 ± 0.0002 Å
c	16.0701 ± 0.0003 Å
α	91.602 ± 0.002°
β	95.622 ± 0.002°
γ	115.21 ± 0.002°
Cell volume	1740 ± 0.06 Å³
Cell temperature	113 ± 2 K
Ambient diffraction temperature	113 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0302
Residual factor for significantly intense reflections	0.0226
Weighted residual factors for significantly intense reflections	0.0516
Weighted residual factors for all reflections included in the refinement	0.0532
Goodness-of-fit parameter for all reflections included in the refinement	1.018
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179104 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/66.	4306611.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4306611.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4306611.cif
1167	2010-05-13	cif/ Adding data from the rest of 2009 RSC journals, Inorg-Chem-2008 and Chem-Comm-2010_18-19.	4306611.cif