Crystallography Open Database

Information card for entry 4306616

Preview

Coordinates	4306616.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Gd(^i^PrN)~2~CN^i^Pr~2~ (3b)
Formula	C45 H96 Gd N9
Calculated formula	C45 H96 Gd N9
SMILES	C1(=[N](C(C)C)[Gd]23(N1C(C)C)([N](=C(N3C(C)C)N(C(C)C)C(C)C)C(C)C)[N](=C(N2C(C)C)N(C(C)C)C(C)C)C(C)C)N(C(C)C)C(C)C.C1CCCCC1
Title of publication	Synthesis, Characterization, and Thermal Properties of Homoleptic Rare-Earth Guanidinates: Promising Precursors for MOCVD and ALD of Rare-Earth Oxide Thin Films
Authors of publication	Andrian P. Milanov; Roland A. Fischer; Anjana Devi
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	11405 - 11416
a	23.0567 ± 0.0013 Å
b	13.2892 ± 0.0006 Å
c	19.4508 ± 0.0009 Å
α	90°
β	118.558 ± 0.005°
γ	90°
Cell volume	5234.7 ± 0.5 Å³
Cell temperature	113 ± 2 K
Ambient diffraction temperature	113 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.034
Residual factor for significantly intense reflections	0.0265
Weighted residual factors for significantly intense reflections	0.0592
Weighted residual factors for all reflections included in the refinement	0.0602
Goodness-of-fit parameter for all reflections included in the refinement	0.956
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179104 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/66.	4306616.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4306616.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4306616.cif
1167	2010-05-13	cif/ Adding data from the rest of 2009 RSC journals, Inorg-Chem-2008 and Chem-Comm-2010_18-19.	4306616.cif