Crystallography Open Database

Information card for entry 4306683

Preview

Coordinates	4306683.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	2,3-bis-(trimethylsilyl)-4,4-bis-(trimethylsilyl)-cyclo-2-phospha-4-sila-2,3- diazenium tetrachlorogallate
Formula	C12 H36 Cl4 Ga N2 P Si5
Calculated formula	C12 H36 Cl4 Ga N2 P Si5
Title of publication	GaCl3-Assisted Cyclization Reactions in Hypersilyl(trimethylsilyl)aminodichlorophosphine
Authors of publication	Alexander Villinger; Andrea Westenkirchner; Ronald Wustrack; Axel Schulz
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	9140 - 9142
a	16.101 ± 0.003 Å
b	12.561 ± 0.003 Å
c	18.617 ± 0.007 Å
α	90°
β	125.069 ± 0.018°
γ	90°
Cell volume	3081.7 ± 1.6 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0443
Residual factor for significantly intense reflections	0.0266
Weighted residual factors for significantly intense reflections	0.0638
Weighted residual factors for all reflections included in the refinement	0.0705
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179104 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/66.	4306683.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4306683.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4306683.cif
1167	2010-05-13	cif/ Adding data from the rest of 2009 RSC journals, Inorg-Chem-2008 and Chem-Comm-2010_18-19.	4306683.cif