Crystallography Open Database

Information card for entry 4306703

Preview

Coordinates	4306703.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	N-(trifluoromethylsulfonatodimethylsilyl)-N-[bis-(2,4,6-trimethylphenyl)phenyl] amino-trifluoromethylsulfonatomethylarsane toluene solvate
Formula	C36 H42 As F6 N O6 S2 Si
Calculated formula	C36 H42 As F6 N O6 S2 Si
Title of publication	Lewis-Acid-Assisted Methyl Exchange Reactions In Silylated Aminodichloroarsanes
Authors of publication	Dirk Michalik; Axel Schulz; Alexander Villinger
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	11798 - 11806
a	12.241 ± 0.002 Å
b	20.94 ± 0.004 Å
c	15.639 ± 0.003 Å
α	90°
β	99.51 ± 0.03°
γ	90°
Cell volume	3953.6 ± 1.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0588
Residual factor for significantly intense reflections	0.0405
Weighted residual factors for significantly intense reflections	0.1108
Weighted residual factors for all reflections included in the refinement	0.1189
Goodness-of-fit parameter for all reflections included in the refinement	1.065
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179105 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/67.	4306703.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4306703.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4306703.cif
1167	2010-05-13	cif/ Adding data from the rest of 2009 RSC journals, Inorg-Chem-2008 and Chem-Comm-2010_18-19.	4306703.cif