Crystallography Open Database

Information card for entry 4306941

Preview

Coordinates	4306941.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	complex 2
Formula	C32 H29 B2 F8 N9 Ru
Calculated formula	C32 H29 B2 F7.92 N9 Ru
Title of publication	Synthesis of Pd Complexes Combined with Photosensitizing of a Ruthenium(II) Polypyridyl Moiety through a Series of Substituted Bipyrimidine Bridges. Substituent Effect of the Bridging Ligand on the Photocatalytic Dimerization of α-Methylstyrene
Authors of publication	Akiko Inagaki; Shinichi Yatsuda; Shinichi Edure; Akiko Suzuki; Takeshi Takahashi; Munetaka Akita
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	2432 - 2445
a	11.0233 ± 0.0015 Å
b	12.527 ± 0.003 Å
c	13.66 ± 0.003 Å
α	108.132 ± 0.005°
β	100.31 ± 0.009°
γ	98.311 ± 0.011°
Cell volume	1722.8 ± 0.6 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0837
Residual factor for significantly intense reflections	0.0552
Weighted residual factors for significantly intense reflections	0.1337
Weighted residual factors for all reflections included in the refinement	0.1504
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179107 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/69.	4306941.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4306941.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4306941.cif
1194	2010-06-06	cif/4/ Adding data from Inorg-Chem-2007_01-13/ processing directory.	4306941.cif