Crystallography Open Database

Information card for entry 4306943

Preview

Coordinates	4306943.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	complex4
Formula	C33 H32 F12 N8 O P2 Ru
Calculated formula	C33 H26 F11.94 N8 O P2 Ru
Title of publication	Synthesis of Pd Complexes Combined with Photosensitizing of a Ruthenium(II) Polypyridyl Moiety through a Series of Substituted Bipyrimidine Bridges. Substituent Effect of the Bridging Ligand on the Photocatalytic Dimerization of α-Methylstyrene
Authors of publication	Akiko Inagaki; Shinichi Yatsuda; Shinichi Edure; Akiko Suzuki; Takeshi Takahashi; Munetaka Akita
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	2432 - 2445
a	13.247 ± 0.003 Å
b	23.613 ± 0.006 Å
c	12.127 ± 0.003 Å
α	90°
β	99.452 ± 0.018°
γ	90°
Cell volume	3741.8 ± 1.6 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/a 1
Hall space group symbol	-P 2yab
Residual factor for all reflections	0.0677
Residual factor for significantly intense reflections	0.0511
Weighted residual factors for significantly intense reflections	0.1392
Weighted residual factors for all reflections included in the refinement	0.1499
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179107 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/69.	4306943.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4306943.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4306943.cif
1194	2010-06-06	cif/4/ Adding data from Inorg-Chem-2007_01-13/ processing directory.	4306943.cif