Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4306956
Preview
| Coordinates | 4306956.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | (dimethylsilyl)(dimethylchlorosilyl)niobocene hydrid |
|---|---|
| Chemical name | bis(cyclopentadienyl)(dimethylsilyl) (dimethylchlorosilyl)(hydrido) niobium (V) |
| Formula | C14 H24 Cl Nb Si2 |
| Calculated formula | C14 H24 Cl Nb Si2 |
| Title of publication | Syntheses and Structures of Asymmetric Bis(silyl) Niobocene Hydrides |
| Authors of publication | Konstantin Yu. Dorogov; Muhammed Yousufuddin; Nam-Nhat Ho; Andrei V. Churakov; Lyudmila G. Kuzmina; Arthur J. Schultz; Sax A. Mason; Judith A. K. Howard; Dmitry A. Lemenovskii; Robert Bau; Georgii I. Nikonov |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2007 |
| Journal volume | 46 |
| Pages of publication | 147 - 160 |
| a | 13.6876 ± 0.0004 Å |
| b | 8.5767 ± 0.0003 Å |
| c | 14.5354 ± 0.0004 Å |
| α | 90° |
| β | 93.627 ± 0.002° |
| γ | 90° |
| Cell volume | 1702.96 ± 0.09 Å3 |
| Cell temperature | 120 ± 0.2 K |
| Ambient diffraction temperature | 120 ± 0.2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0266 |
| Residual factor for significantly intense reflections | 0.0247 |
| Weighted residual factors for significantly intense reflections | 0.0677 |
| Weighted residual factors for all reflections included in the refinement | 0.0691 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.155 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179107 (current) | 2016-03-23 | cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/69. |
4306956.cif |
| 120081 | 2014-07-12 | Adding DOIs to range 4/30 structures. | 4306956.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4306956.cif |
| 1194 | 2010-06-06 | cif/4/ Adding data from Inorg-Chem-2007_01-13/ processing directory. |
4306956.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.