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Information card for entry 4306963
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| Coordinates | 4306963.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | (dimethylbromosilyl)(dimethylchlorosilyl)niobocene hydrid |
|---|---|
| Chemical name | bis(cyclopentadienyl)(dimethylbromosilyl) (dimethylchlorosilyl)(hydrido) niobium (V) |
| Formula | C14 H23 Br Cl Nb Si2 |
| Calculated formula | C14 H23 Br0.9526 Cl1.0474 Nb Si2 |
| Title of publication | Syntheses and Structures of Asymmetric Bis(silyl) Niobocene Hydrides |
| Authors of publication | Konstantin Yu. Dorogov; Muhammed Yousufuddin; Nam-Nhat Ho; Andrei V. Churakov; Lyudmila G. Kuzmina; Arthur J. Schultz; Sax A. Mason; Judith A. K. Howard; Dmitry A. Lemenovskii; Robert Bau; Georgii I. Nikonov |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2007 |
| Journal volume | 46 |
| Pages of publication | 147 - 160 |
| a | 16.6006 ± 0.0005 Å |
| b | 13.1582 ± 0.0004 Å |
| c | 8.4922 ± 0.0002 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 1854.99 ± 0.09 Å3 |
| Cell temperature | 123 ± 2 K |
| Ambient diffraction temperature | 123 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 62 |
| Hermann-Mauguin space group symbol | P n m a |
| Hall space group symbol | -P 2ac 2n |
| Residual factor for all reflections | 0.0228 |
| Residual factor for significantly intense reflections | 0.0176 |
| Weighted residual factors for significantly intense reflections | 0.0404 |
| Weighted residual factors for all reflections included in the refinement | 0.0419 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.029 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179107 (current) | 2016-03-23 | cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/69. |
4306963.cif |
| 120081 | 2014-07-12 | Adding DOIs to range 4/30 structures. | 4306963.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4306963.cif |
| 1194 | 2010-06-06 | cif/4/ Adding data from Inorg-Chem-2007_01-13/ processing directory. |
4306963.cif |
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Users of the data should acknowledge the original authors of the
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