Crystallography Open Database

Information card for entry 4307385

Preview

Coordinates	4307385.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C17 H37 Cl5 N8 Pt
Calculated formula	C17 H37 Cl5 N8 Pt
Title of publication	PtII-Mediated Nitrile-Tetramethylguanidine Coupling as a Key Step for a Novel Synthesis of 1,6-Dihydro-1,3,5-triazines
Authors of publication	Pavel V. Gushchin; Nadezhda A. Bokach; Konstantin V. Luzyanin; Alexey A. Nazarov; Matti Haukka; Vadim Yu. Kukushkin
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	1684 - 1693
a	19.0947 ± 0.0011 Å
b	12.4624 ± 0.0008 Å
c	12.5981 ± 0.0006 Å
α	90°
β	107.268 ± 0.004°
γ	90°
Cell volume	2862.8 ± 0.3 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0422
Residual factor for significantly intense reflections	0.0303
Weighted residual factors for significantly intense reflections	0.058
Weighted residual factors for all reflections included in the refinement	0.061
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179111 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/73.	4307385.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4307385.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4307385.cif
1194	2010-06-06	cif/4/ Adding data from Inorg-Chem-2007_01-13/ processing directory.	4307385.cif