Crystallography Open Database

Information card for entry 4307763

Preview

Coordinates	4307763.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C82 H100.4 N26 Ni7 O32.2
Calculated formula	C82 H76 N26 Ni7 O32.2
Title of publication	Acetate/Di-2-pyridyl Ketone Oximate "Blend" as a Source of High-Nuclearity Nickel(II) Clusters: Dependence of the Nuclearity on the Nature of the Inorganic Anion Present
Authors of publication	Theocharis C. Stamatatos; Eleanna Diamantopoulou; Catherine P. Raptopoulou; Vassilis Psycharis; Albert Escuer; Spyros P. Perlepes
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	2350 - 2352
a	21.475 ± 0.009 Å
b	21.955 ± 0.009 Å
c	11.352 ± 0.005 Å
α	90°
β	96.393 ± 0.012°
γ	90°
Cell volume	5319 ± 4 Å³
Cell temperature	298 K
Ambient diffraction temperature	298 K
Number of distinct elements	5
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/a 1
Hall space group symbol	-P 2ya
Residual factor for all reflections	0.0723
Residual factor for significantly intense reflections	0.0453
Weighted residual factors for significantly intense reflections	0.115
Weighted residual factors for all reflections included in the refinement	0.1307
Goodness-of-fit parameter for all reflections included in the refinement	1.099
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179115 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/77.	4307763.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4307763.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4307763.cif
1194	2010-06-06	cif/4/ Adding data from Inorg-Chem-2007_01-13/ processing directory.	4307763.cif