Crystallography Open Database

Information card for entry 4307796

Preview

Coordinates	4307796.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H46 B2 Li N4 Sb
Calculated formula	C28 H46 B2 Li N4 Sb
Title of publication	New Bonding Modes for Boraamidinate Ligands in Heavy Group 15 Complexes: Fluxional Behavior of the 1:2 Complexes, LiM[PhB(NtBu)2]2 (M = As, Sb, Bi)
Authors of publication	Jari Konu; Maravanji S. Balakrishna; Tristram Chivers; Thomas W. Swaddle
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	2627 - 2636
a	25.878 ± 0.005 Å
b	8.7115 ± 0.0017 Å
c	18.521 ± 0.004 Å
α	90°
β	133.85 ± 0.03°
γ	90°
Cell volume	3011 ± 1.8 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.116
Residual factor for significantly intense reflections	0.0662
Weighted residual factors for significantly intense reflections	0.126
Weighted residual factors for all reflections included in the refinement	0.1419
Goodness-of-fit parameter for all reflections included in the refinement	1.061
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179115 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/77.	4307796.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4307796.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4307796.cif
1194	2010-06-06	cif/4/ Adding data from Inorg-Chem-2007_01-13/ processing directory.	4307796.cif