Crystallography Open Database

Information card for entry 4308069

Preview

Coordinates	4308069.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H54 B2 F4 N2 P2
Calculated formula	C24 H54 B1.98 F4.02 N2 P2
Title of publication	Boron and Aluminum Complexes of Sterically Demanding Phosphinimines and Phosphinimides
Authors of publication	Silke Courtenay; Denise Walsh; Sarah Hawkeswood; Pingrong Wei; Anjan Kumar Das; Douglas W. Stephan
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	3623 - 3631
a	14.298 ± 0.004 Å
b	14.298 ± 0.004 Å
c	14.298 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	2923 ± 1.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	205
Hermann-Mauguin space group symbol	P a -3
Hall space group symbol	-P 2ac 2ab 3
Residual factor for all reflections	0.0802
Residual factor for significantly intense reflections	0.0588
Weighted residual factors for significantly intense reflections	0.1571
Weighted residual factors for all reflections included in the refinement	0.1757
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179118 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/80.	4308069.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4308069.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4308069.cif
1194	2010-06-06	cif/4/ Adding data from Inorg-Chem-2007_01-13/ processing directory.	4308069.cif