#------------------------------------------------------------------------------
#$Date: 2016-03-23 00:41:36 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179123 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/85/4308557.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4308557
loop_
_publ_author_name
'Rodney P. Feazell'
'Cody E. Carson'
'Kevin K. Klausmeyer'
_publ_section_title
;
Anion-Dependent Silver(I) Coordination Polymers of the Tridentate
Pyridylphosphonite: PPh(3-OCH2C5H4N)2
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              996
_journal_page_last               1005
_journal_paper_doi               10.1021/ic0486365
_journal_volume                  44
_journal_year                    2005
_chemical_formula_moiety
'C72 H68 Ag4 B F4 N8 O8 P4, 3(B F4), 4(C2 H3 N)'
_chemical_formula_sum            'C80 H80 Ag4 B4 F16 N12 O8 P4'
_chemical_formula_weight         2240.16
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           19
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   15.565(2)
_cell_length_b                   20.999(3)
_cell_length_c                   28.131(4)
_cell_measurement_reflns_used    6479
_cell_measurement_temperature    110(2)
_cell_measurement_theta_max      19.00
_cell_measurement_theta_min      2.34
_cell_volume                     9195(2)
_computing_cell_refinement       'Bruker APEX2'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINTPLUS'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      110(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0836
_diffrn_reflns_av_sigmaI/netI    0.0802
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_limit_l_min       -31
_diffrn_reflns_number            67540
_diffrn_reflns_theta_full        23.26
_diffrn_reflns_theta_max         23.26
_diffrn_reflns_theta_min         1.21
_exptl_absorpt_coefficient_mu    1.000
_exptl_absorpt_correction_T_max  0.9601
_exptl_absorpt_correction_T_min  0.8507
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.618
_exptl_crystal_density_meas      0
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             4480
_exptl_crystal_size_max          0.167
_exptl_crystal_size_mid          0.140
_exptl_crystal_size_min          0.041
_refine_diff_density_max         0.995
_refine_diff_density_min         -0.641
_refine_diff_density_rms         0.102
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.00(3)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.112
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1147
_refine_ls_number_reflns         13167
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.112
_refine_ls_R_factor_all          0.0542
_refine_ls_R_factor_gt           0.0463
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0000P)²+25.0027P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1123
_refine_ls_wR_factor_ref         0.1174
_reflns_number_gt                11926
_reflns_number_total             13167
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic0486365si20040928_045440_3.cif
_cod_data_source_block           kk44
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4308557
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.84735(4) 0.61241(2) 0.12944(2) 0.02387(15) Uani 1 1 d . . .
Ag2 Ag 0.34538(4) 0.37350(3) 0.13544(2) 0.02440(15) Uani 1 1 d . . .
Ag3 Ag -0.17467(4) 0.14210(2) 0.11810(2) 0.02586(16) Uani 1 1 d . . .
Ag4 Ag -0.67814(3) -0.12176(3) 0.11841(2) 0.02373(15) Uani 1 1 d . . .
B1 B 0.4838(7) 0.3324(5) 0.7525(4) 0.034(2) Uani 1 1 d . . .
B2 B 0.7414(6) 0.1448(4) 0.9945(3) 0.027(2) Uani 0.512(5) 1 d P A 1
B3 B 1.0000(6) 0.5860(5) 0.7693(4) 0.031(2) Uani 1 1 d . . .
B4 B 0.7791(6) 0.3766(5) 0.5087(3) 0.024(2) Uani 0.504(8) 1 d P B 1
B2A B 0.7414(6) 0.1448(4) 0.9945(3) 0.027(2) Uani 0.488(5) 1 d P A 2
B4A B 0.7791(6) 0.3766(5) 0.5087(3) 0.024(2) Uani 0.496(8) 1 d P B 2
C1 C 1.1363(5) 0.7724(4) 0.1188(3) 0.036(2) Uani 1 1 d . . .
H1A H 1.1460 0.8139 0.1031 0.043 Uiso 1 1 calc R . .
H1B H 1.1118 0.7802 0.1508 0.043 Uiso 1 1 calc R . .
C2 C 1.0756(5) 0.7315(3) 0.0894(3) 0.0247(18) Uani 1 1 d . . .
C3 C 1.0118(5) 0.6968(3) 0.1119(3) 0.0216(17) Uani 1 1 d . . .
H3 H 1.0075 0.6988 0.1456 0.026 Uiso 1 1 calc R . .
C4 C 0.9634(6) 0.6571(4) 0.0405(3) 0.034(2) Uani 1 1 d . . .
H4 H 0.9237 0.6319 0.0231 0.041 Uiso 1 1 calc R . .
C5 C 1.0272(6) 0.6893(4) 0.0162(3) 0.041(2) Uani 1 1 d . . .
H5 H 1.0332 0.6844 -0.0172 0.049 Uiso 1 1 calc R . .
C6 C 1.0807(6) 0.7278(4) 0.0406(3) 0.038(2) Uani 1 1 d . . .
H6 H 1.1221 0.7526 0.0240 0.045 Uiso 1 1 calc R . .
C7 C 0.7298(6) 0.7368(4) 0.1249(3) 0.039(2) Uani 1 1 d . . .
H7 H 0.7216 0.7226 0.0932 0.047 Uiso 1 1 calc R . .
C8 C 0.6797(7) 0.7887(4) 0.1414(3) 0.048(3) Uani 1 1 d . . .
H8 H 0.6375 0.8078 0.1216 0.057 Uiso 1 1 calc R . .
C9 C 0.6935(6) 0.8103(4) 0.1863(3) 0.041(2) Uani 1 1 d . . .
H9 H 0.6606 0.8449 0.1984 0.049 Uiso 1 1 calc R . .
C10 C 0.7565(5) 0.7814(3) 0.2149(3) 0.0252(18) Uani 1 1 d . . .
C11 C 0.8004(5) 0.7300(4) 0.1948(3) 0.0256(19) Uani 1 1 d . . .
H11 H 0.8431 0.7096 0.2135 0.031 Uiso 1 1 calc R . .
C12 C 0.9068(5) 0.4487(4) 0.1395(3) 0.0251(18) Uani 1 1 d . . .
C13 C 0.9073(5) 0.3874(4) 0.1587(3) 0.033(2) Uani 1 1 d . . .
H13 H 0.8632 0.3757 0.1803 0.040 Uiso 1 1 calc R . .
C14 C 0.9679(5) 0.3442(4) 0.1476(3) 0.034(2) Uani 1 1 d . . .
H14 H 0.9655 0.3022 0.1599 0.041 Uiso 1 1 calc R . .
C15 C 1.0372(6) 0.3638(4) 0.1163(3) 0.042(2) Uani 1 1 d . . .
H15 H 1.0838 0.3359 0.1099 0.050 Uiso 1 1 calc R . .
C16 C 1.0343(6) 0.4218(4) 0.0966(3) 0.037(2) Uani 1 1 d . . .
H16 H 1.0767 0.4329 0.0738 0.044 Uiso 1 1 calc R . .
C17 C 0.9723(5) 0.4663(3) 0.1080(3) 0.0269(19) Uani 1 1 d . . .
H17 H 0.9741 0.5079 0.0949 0.032 Uiso 1 1 calc R . .
C18 C 0.7894(5) 0.5477(3) 0.2427(3) 0.0254(18) Uani 1 1 d . . .
H18A H 0.7267 0.5526 0.2378 0.030 Uiso 1 1 calc R . .
H18B H 0.8175 0.5891 0.2360 0.030 Uiso 1 1 calc R . .
C19 C 0.6602(5) 0.5046(4) 0.1384(3) 0.033(2) Uani 1 1 d . . .
H19A H 0.6674 0.5495 0.1285 0.040 Uiso 1 1 calc R . .
H19B H 0.6392 0.5040 0.1716 0.040 Uiso 1 1 calc R . .
C20 C 0.5976(5) 0.4715(3) 0.1064(3) 0.0245(19) Uani 1 1 d . . .
C21 C 0.5217(5) 0.4471(3) 0.1254(3) 0.0239(17) Uani 1 1 d . . .
H21 H 0.5129 0.4505 0.1588 0.029 Uiso 1 1 calc R . .
C22 C 0.4751(5) 0.4130(4) 0.0516(3) 0.0281(19) Uani 1 1 d . . .
H22 H 0.4324 0.3938 0.0323 0.034 Uiso 1 1 calc R . .
C23 C 0.5506(5) 0.4340(4) 0.0307(3) 0.0245(18) Uani 1 1 d . . .
H23 H 0.5602 0.4277 -0.0023 0.029 Uiso 1 1 calc R . .
C24 C 0.6121(5) 0.4644(4) 0.0586(3) 0.0289(19) Uani 1 1 d . . .
H24 H 0.6636 0.4801 0.0447 0.035 Uiso 1 1 calc R . .
C25 C 0.2241(5) 0.4964(4) 0.1416(3) 0.034(2) Uani 1 1 d . . .
H25 H 0.2138 0.4837 0.1097 0.040 Uiso 1 1 calc R . .
C26 C 0.1786(6) 0.5472(4) 0.1589(3) 0.041(2) Uani 1 1 d . . .
H26 H 0.1378 0.5686 0.1395 0.049 Uiso 1 1 calc R . .
C27 C 0.1931(5) 0.5667(4) 0.2050(3) 0.036(2) Uani 1 1 d . . .
H27 H 0.1628 0.6018 0.2180 0.043 Uiso 1 1 calc R . .
C28 C 0.2544(5) 0.5332(3) 0.2324(3) 0.0222(17) Uani 1 1 d . . .
C29 C 0.2954(5) 0.4822(4) 0.2116(3) 0.030(2) Uani 1 1 d . . .
H29 H 0.3357 0.4587 0.2300 0.036 Uiso 1 1 calc R . .
C30 C 0.3786(5) 0.2028(4) 0.1421(3) 0.0278(19) Uani 1 1 d . . .
C31 C 0.3784(6) 0.1476(4) 0.1706(3) 0.036(2) Uani 1 1 d . . .
H31 H 0.3362 0.1425 0.1947 0.043 Uiso 1 1 calc R . .
C32 C 0.4392(6) 0.1014(4) 0.1636(4) 0.042(2) Uani 1 1 d . . .
H32 H 0.4381 0.0640 0.1827 0.050 Uiso 1 1 calc R . .
C33 C 0.5006(7) 0.1083(4) 0.1301(4) 0.062(3) Uani 1 1 d . . .
H33 H 0.5448 0.0773 0.1272 0.075 Uiso 1 1 calc R . .
C34 C 0.4993(7) 0.1608(5) 0.0996(4) 0.058(3) Uani 1 1 d . . .
H34 H 0.5399 0.1642 0.0745 0.069 Uiso 1 1 calc R . .
C35 C 0.4374(6) 0.2084(4) 0.1064(3) 0.042(2) Uani 1 1 d . . .
H35 H 0.4365 0.2446 0.0861 0.051 Uiso 1 1 calc R . .
C36 C 0.2322(6) 0.2979(4) 0.2344(3) 0.033(2) Uani 1 1 d . . .
H36A H 0.1708 0.2951 0.2255 0.040 Uiso 1 1 calc R . .
H36B H 0.2523 0.3419 0.2285 0.040 Uiso 1 1 calc R . .
C37 C 0.1786(5) 0.1897(3) 0.1239(3) 0.0270(18) Uani 1 1 d . . .
H37A H 0.1622 0.1784 0.1568 0.032 Uiso 1 1 calc R . .
H37B H 0.2184 0.1568 0.1116 0.032 Uiso 1 1 calc R . .
C38 C 0.0994(5) 0.1944(4) 0.0924(3) 0.0252(18) Uani 1 1 d . . .
C39 C 0.0207(5) 0.1775(3) 0.1092(3) 0.0272(19) Uani 1 1 d . . .
H39 H 0.0175 0.1619 0.1409 0.033 Uiso 1 1 calc R . .
C40 C -0.0463(5) 0.2044(4) 0.0403(3) 0.0276(19) Uani 1 1 d . . .
H40 H -0.0969 0.2072 0.0216 0.033 Uiso 1 1 calc R . .
C41 C 0.0308(5) 0.2249(4) 0.0202(3) 0.032(2) Uani 1 1 d . . .
H41 H 0.0322 0.2419 -0.0111 0.038 Uiso 1 1 calc R . .
C42 C 0.1048(5) 0.2199(4) 0.0467(3) 0.0291(19) Uani 1 1 d . . .
H42 H 0.1584 0.2335 0.0342 0.035 Uiso 1 1 calc R . .
C43 C -0.3133(6) 0.2544(4) 0.1274(3) 0.044(2) Uani 1 1 d . . .
H43 H -0.3256 0.2422 0.0956 0.053 Uiso 1 1 calc R . .
C44 C -0.3634(7) 0.2994(5) 0.1482(4) 0.060(3) Uani 1 1 d . . .
H44 H -0.4097 0.3178 0.1310 0.071 Uiso 1 1 calc R . .
C45 C -0.3474(6) 0.3184(4) 0.1938(4) 0.051(3) Uani 1 1 d . . .
H45 H -0.3824 0.3498 0.2086 0.061 Uiso 1 1 calc R . .
C46 C -0.2790(5) 0.2911(4) 0.2181(3) 0.031(2) Uani 1 1 d . . .
C47 C -0.2325(5) 0.2454(4) 0.1951(3) 0.0267(19) Uani 1 1 d . . .
H47 H -0.1869 0.2256 0.2120 0.032 Uiso 1 1 calc R . .
C48 C -0.1408(5) -0.0271(3) 0.1091(3) 0.0221(17) Uani 1 1 d . . .
C49 C -0.1263(5) -0.0854(4) 0.1314(3) 0.0308(19) Uani 1 1 d . . .
H49 H -0.1555 -0.0950 0.1601 0.037 Uiso 1 1 calc R . .
C50 C -0.0704(5) -0.1293(4) 0.1123(3) 0.033(2) Uani 1 1 d . . .
H50 H -0.0594 -0.1680 0.1288 0.040 Uiso 1 1 calc R . .
C51 C -0.0297(5) -0.1175(4) 0.0692(3) 0.039(2) Uani 1 1 d . . .
H51 H 0.0066 -0.1486 0.0551 0.046 Uiso 1 1 calc R . .
C52 C -0.0433(6) -0.0593(4) 0.0471(3) 0.035(2) Uani 1 1 d . . .
H52 H -0.0146 -0.0504 0.0180 0.043 Uiso 1 1 calc R . .
C53 C -0.0977(5) -0.0142(4) 0.0664(3) 0.029(2) Uani 1 1 d . . .
H53 H -0.1059 0.0254 0.0507 0.034 Uiso 1 1 calc R . .
C54 C -0.2731(5) 0.0510(4) 0.2168(3) 0.031(2) Uani 1 1 d . . .
H54A H -0.3351 0.0456 0.2102 0.037 Uiso 1 1 calc R . .
H54B H -0.2579 0.0962 0.2114 0.037 Uiso 1 1 calc R . .
C55 C -0.3339(5) -0.0429(4) 0.0971(3) 0.035(2) Uani 1 1 d . . .
H55A H -0.3359 -0.0669 0.1274 0.042 Uiso 1 1 calc R . .
H55B H -0.2957 -0.0658 0.0747 0.042 Uiso 1 1 calc R . .
C56 C -0.4234(5) -0.0364(4) 0.0763(3) 0.0256(18) Uani 1 1 d . . .
C57 C -0.4908(5) -0.0706(3) 0.0968(3) 0.0217(17) Uani 1 1 d . . .
H57 H -0.4783 -0.0984 0.1226 0.026 Uiso 1 1 calc R . .
C58 C -0.5898(5) -0.0252(4) 0.0466(3) 0.033(2) Uani 1 1 d . . .
H58 H -0.6479 -0.0190 0.0373 0.039 Uiso 1 1 calc R . .
C59 C -0.5248(6) 0.0089(4) 0.0230(3) 0.040(2) Uani 1 1 d . . .
H59 H -0.5382 0.0351 -0.0035 0.047 Uiso 1 1 calc R . .
C60 C -0.4406(5) 0.0035(4) 0.0389(3) 0.033(2) Uani 1 1 d . . .
H60 H -0.3958 0.0271 0.0243 0.040 Uiso 1 1 calc R . .
C61 C -0.8357(5) -0.0204(3) 0.1181(3) 0.0310(19) Uani 1 1 d . . .
H61 H -0.8471 -0.0379 0.0875 0.037 Uiso 1 1 calc R . .
C62 C -0.8933(6) 0.0211(4) 0.1376(3) 0.032(2) Uani 1 1 d . . .
H62 H -0.9418 0.0347 0.1198 0.039 Uiso 1 1 calc R . .
C63 C -0.8810(5) 0.0431(4) 0.1830(3) 0.0279(19) Uani 1 1 d . . .
H63 H -0.9232 0.0693 0.1976 0.033 Uiso 1 1 calc R . .
C64 C -0.8078(5) 0.0272(3) 0.2074(3) 0.0234(18) Uani 1 1 d . . .
C65 C -0.7499(5) -0.0132(3) 0.1846(3) 0.0225(18) Uani 1 1 d . . .
H65 H -0.6985 -0.0242 0.2008 0.027 Uiso 1 1 calc R . .
C66 C -0.6209(5) -0.2867(3) 0.1245(3) 0.0256(18) Uani 1 1 d . . .
C67 C -0.6312(6) -0.3502(4) 0.1344(4) 0.053(3) Uani 1 1 d . . .
H67 H -0.6793 -0.3639 0.1525 0.064 Uiso 1 1 calc R . .
C68 C -0.5720(7) -0.3950(4) 0.1181(4) 0.060(3) Uani 1 1 d . . .
H68 H -0.5773 -0.4387 0.1263 0.072 Uiso 1 1 calc R . .
C69 C -0.5076(6) -0.3746(4) 0.0907(3) 0.036(2) Uani 1 1 d . . .
H69 H -0.4699 -0.4052 0.0771 0.043 Uiso 1 1 calc R . .
C70 C -0.4940(6) -0.3131(5) 0.0818(4) 0.057(3) Uani 1 1 d . . .
H70 H -0.4448 -0.2999 0.0645 0.068 Uiso 1 1 calc R . .
C71 C -0.5516(6) -0.2694(4) 0.0979(4) 0.048(3) Uani 1 1 d . . .
H71 H -0.5433 -0.2258 0.0904 0.057 Uiso 1 1 calc R . .
C72 C -0.7402(6) -0.1920(4) 0.2306(3) 0.038(2) Uani 1 1 d . . .
H72A H -0.8030 -0.1912 0.2253 0.046 Uiso 1 1 calc R . .
H72B H -0.7169 -0.1492 0.2232 0.046 Uiso 1 1 calc R . .
C73 C 0.7095(9) 0.1613(8) 0.4913(5) 0.091(5) Uani 1 1 d . . .
H73A H 0.7252 0.1728 0.5239 0.137 Uiso 1 1 calc R . .
H73B H 0.6495 0.1474 0.4905 0.137 Uiso 1 1 calc R . .
H73C H 0.7168 0.1984 0.4705 0.137 Uiso 1 1 calc R . .
C74 C 0.7654(12) 0.1092(8) 0.4746(6) 0.094(5) Uani 1 1 d . . .
C75 C 0.3180(9) 0.1489(5) 0.9589(5) 0.085(4) Uani 1 1 d . . .
H75A H 0.2940 0.1286 0.9305 0.128 Uiso 1 1 calc R . .
H75B H 0.3807 0.1451 0.9585 0.128 Uiso 1 1 calc R . .
H75C H 0.3018 0.1940 0.9594 0.128 Uiso 1 1 calc R . .
C76 C 0.2844(7) 0.1176(5) 1.0011(4) 0.051(3) Uani 1 1 d . . .
C77 C 0.9971(7) 0.2817(5) 0.7381(4) 0.059(3) Uani 1 1 d . . .
H77A H 0.9851 0.2770 0.7722 0.089 Uiso 1 1 calc R . .
H77B H 1.0566 0.2957 0.7337 0.089 Uiso 1 1 calc R . .
H77C H 0.9886 0.2407 0.7222 0.089 Uiso 1 1 calc R . .
C78 C 0.9377(6) 0.3299(5) 0.7174(4) 0.044(2) Uani 1 1 d . . .
C79 C 0.5389(6) 0.0423(5) 0.7520(4) 0.051(3) Uani 1 1 d . . .
H79A H 0.5031 0.0077 0.7644 0.076 Uiso 1 1 calc R . .
H79B H 0.5717 0.0614 0.7781 0.076 Uiso 1 1 calc R . .
H79C H 0.5787 0.0254 0.7281 0.076 Uiso 1 1 calc R . .
C80 C 0.4846(6) 0.0904(5) 0.7303(4) 0.044(2) Uani 1 1 d . . .
F1 F 0.4375(3) 0.3672(2) 0.78631(17) 0.0376(12) Uani 1 1 d . . .
F2 F 0.5231(3) 0.3727(2) 0.72092(17) 0.0405(12) Uani 1 1 d . . .
F3 F 0.5465(3) 0.2959(3) 0.77630(18) 0.0481(14) Uani 1 1 d . . .
F4 F 0.4273(3) 0.2929(2) 0.72776(18) 0.0427(13) Uani 1 1 d . . .
F5 F 0.7807(7) 0.2036(6) 0.9829(4) 0.0538(12) Uani 0.512(5) 1 d P A 1
F6 F 0.6560(7) 0.1455(5) 1.0099(4) 0.0538(12) Uani 0.512(5) 1 d P A 1
F7 F 0.7352(7) 0.1166(5) 0.9484(4) 0.0538(12) Uani 0.512(5) 1 d P A 1
F8 F 0.7966(13) 0.1070(9) 1.0208(8) 0.0538(12) Uani 0.512(5) 1 d P A 1
F9 F 0.9624(4) 0.6295(3) 0.79874(18) 0.0561(16) Uani 1 1 d . . .
F10 F 1.0601(3) 0.5502(2) 0.79489(17) 0.0414(13) Uani 1 1 d . . .
F11 F 0.9373(3) 0.5449(3) 0.7501(2) 0.0600(17) Uani 1 1 d . . .
F12 F 1.0407(3) 0.6166(2) 0.73170(16) 0.0348(11) Uani 1 1 d . . .
F13 F 0.7483(9) 0.3117(6) 0.5070(4) 0.0557(12) Uani 0.504(8) 1 d P B 1
F14 F 0.8668(8) 0.3721(7) 0.5155(4) 0.0557(12) Uani 0.504(8) 1 d P B 1
F15 F 0.7648(9) 0.4007(7) 0.4644(4) 0.0557(12) Uani 0.504(8) 1 d P B 1
F16 F 0.7290(9) 0.4158(7) 0.5376(5) 0.0557(12) Uani 0.504(8) 1 d P B 1
F5A F 0.7322(7) 0.1918(6) 1.0306(4) 0.0538(12) Uani 0.488(5) 1 d P A 2
F6A F 0.6574(7) 0.1275(6) 0.9815(4) 0.0538(12) Uani 0.488(5) 1 d P A 2
F7A F 0.7896(8) 0.1715(6) 0.9602(4) 0.0538(12) Uani 0.488(5) 1 d P A 2
F8A F 0.7843(14) 0.0957(10) 1.0160(8) 0.0538(12) Uani 0.488(5) 1 d P A 2
F13A F 0.7900(9) 0.3142(6) 0.5247(5) 0.0557(12) Uani 0.496(8) 1 d P B 2
F14A F 0.8655(8) 0.3992(7) 0.4972(4) 0.0557(12) Uani 0.496(8) 1 d P B 2
F15A F 0.7366(9) 0.3759(7) 0.4683(5) 0.0557(12) Uani 0.496(8) 1 d P B 2
F16A F 0.7495(10) 0.4027(8) 0.5488(5) 0.0557(12) Uani 0.496(8) 1 d P B 2
N1 N 0.9558(4) 0.6604(3) 0.0879(2) 0.0247(15) Uani 1 1 d . . .
N2 N 0.7867(5) 0.7077(3) 0.1511(2) 0.0288(16) Uani 1 1 d . . .
N3 N 0.4604(4) 0.4191(3) 0.0991(2) 0.0220(14) Uani 1 1 d . . .
N4 N 0.2807(4) 0.4641(3) 0.1660(2) 0.0283(16) Uani 1 1 d . . .
N5 N -0.0535(4) 0.1810(3) 0.0843(2) 0.0241(15) Uani 1 1 d . . .
N6 N -0.2473(4) 0.2265(3) 0.1499(2) 0.0274(16) Uani 1 1 d . . .
N7 N -0.5722(4) -0.0660(3) 0.0819(2) 0.0230(15) Uani 1 1 d . . .
N8 N -0.7627(4) -0.0374(3) 0.1410(2) 0.0212(14) Uani 1 1 d . . .
N9 N 0.8126(12) 0.0688(7) 0.4609(5) 0.130(7) Uani 1 1 d . . .
N10 N 0.2528(7) 0.0926(5) 1.0314(3) 0.063(3) Uani 1 1 d . . .
N11 N 0.8904(6) 0.3648(4) 0.7029(3) 0.055(2) Uani 1 1 d . . .
N12 N 0.4403(6) 0.1258(4) 0.7113(3) 0.060(2) Uani 1 1 d . . .
O1 O 1.2167(3) 0.7372(2) 0.1225(2) 0.0295(13) Uani 1 1 d . . .
O2 O 0.7417(3) 0.4709(2) 0.13496(19) 0.0241(12) Uani 1 1 d . . .
O3 O 0.8237(4) 0.4980(2) 0.21129(18) 0.0273(12) Uani 1 1 d . . .
O4 O 0.2191(3) 0.2525(2) 0.1226(2) 0.0271(13) Uani 1 1 d . . .
O5 O 0.2819(4) 0.2535(2) 0.20685(19) 0.0282(13) Uani 1 1 d . . .
O6 O -0.3023(3) 0.0216(2) 0.10517(18) 0.0226(12) Uani 1 1 d . . .
O7 O -0.2226(3) 0.0100(2) 0.18476(19) 0.0249(12) Uani 1 1 d . . .
O8 O -0.7001(3) -0.2399(2) 0.19964(19) 0.0255(12) Uani 1 1 d . . .
P1 P 0.82643(13) 0.50763(9) 0.15482(7) 0.0205(4) Uani 1 1 d . . .
P2 P 0.30437(13) 0.26814(9) 0.15183(7) 0.0228(5) Uani 1 1 d . . .
P3 P -0.21200(12) 0.03440(9) 0.13083(7) 0.0210(4) Uani 1 1 d . . .
P4 P -0.69949(13) -0.22752(9) 0.14322(8) 0.0231(5) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 Ag1 N2 93.2(2) . . ?
N1 Ag1 P1 132.38(16) . . ?
N2 Ag1 P1 133.06(17) . . ?
N3 Ag2 N4 99.4(2) . . ?
N3 Ag2 P2 134.37(16) . . ?
N4 Ag2 P2 125.62(16) . . ?
N5 Ag3 N6 107.3(2) . . ?
N5 Ag3 P3 127.88(16) . . ?
N6 Ag3 P3 124.15(17) . . ?
N7 Ag4 N8 98.3(2) . . ?
N7 Ag4 P4 136.44(16) . . ?
N8 Ag4 P4 124.43(15) . . ?
F2 B1 F4 109.0(8) . . ?
F2 B1 F1 110.4(8) . . ?
F4 B1 F1 109.0(7) . . ?
F2 B1 F3 109.5(8) . . ?
F4 B1 F3 110.5(8) . . ?
F1 B1 F3 108.5(7) . . ?
F8 B2 F6 115.4(12) . . ?
F8 B2 F5 110.8(10) . . ?
F6 B2 F5 118.2(10) . . ?
F8 B2 F7 106.8(11) . . ?
F6 B2 F7 102.8(9) . . ?
F5 B2 F7 100.6(9) . . ?
F9 B3 F12 110.3(8) . . ?
F9 B3 F10 109.5(7) . . ?
F12 B3 F10 109.6(7) . . ?
F9 B3 F11 110.2(7) . . ?
F12 B3 F11 107.9(7) . . ?
F10 B3 F11 109.3(8) . . ?
F15 B4 F14 108.2(9) . . ?
F15 B4 F16 102.9(10) . . ?
F14 B4 F16 120.8(11) . . ?
F15 B4 F13 105.4(10) . . ?
F14 B4 F13 105.6(10) . . ?
F16 B4 F13 112.9(10) . . ?
O1 C1 C2 106.6(6) . . ?
O1 C1 H1A 110.4 . . ?
C2 C1 H1A 110.4 . . ?
O1 C1 H1B 110.4 . . ?
C2 C1 H1B 110.4 . . ?
H1A C1 H1B 108.6 . . ?
C6 C2 C3 117.9(8) . . ?
C6 C2 C1 122.5(7) . . ?
C3 C2 C1 119.5(8) . . ?
N1 C3 C2 122.3(8) . . ?
N1 C3 H3 118.9 . . ?
C2 C3 H3 118.9 . . ?
N1 C4 C5 122.0(8) . . ?
N1 C4 H4 119.0 . . ?
C5 C4 H4 119.0 . . ?
C6 C5 C4 119.1(8) . . ?
C6 C5 H5 120.5 . . ?
C4 C5 H5 120.5 . . ?
C5 C6 C2 120.3(8) . . ?
C5 C6 H6 119.9 . . ?
C2 C6 H6 119.9 . . ?
N2 C7 C8 123.2(9) . . ?
N2 C7 H7 118.4 . . ?
C8 C7 H7 118.4 . . ?
C9 C8 C7 118.4(9) . . ?
C9 C8 H8 120.8 . . ?
C7 C8 H8 120.8 . . ?
C8 C9 C10 119.8(8) . . ?
C8 C9 H9 120.1 . . ?
C10 C9 H9 120.1 . . ?
C11 C10 C9 116.3(7) . . ?
C11 C10 C36 121.0(8) . 3_655 ?
C9 C10 C36 122.2(7) . 3_655 ?
N2 C11 C10 124.5(8) . . ?
N2 C11 H11 117.7 . . ?
C10 C11 H11 117.7 . . ?
C13 C12 C17 119.0(7) . . ?
C13 C12 P1 122.8(6) . . ?
C17 C12 P1 118.2(6) . . ?
C14 C13 C12 122.3(8) . . ?
C14 C13 H13 118.8 . . ?
C12 C13 H13 118.8 . . ?
C13 C14 C15 118.1(8) . . ?
C13 C14 H14 120.9 . . ?
C15 C14 H14 120.9 . . ?
C16 C15 C14 118.8(8) . . ?
C16 C15 H15 120.6 . . ?
C14 C15 H15 120.6 . . ?
C15 C16 C17 123.0(9) . . ?
C15 C16 H16 118.5 . . ?
C17 C16 H16 118.5 . . ?
C16 C17 C12 118.5(8) . . ?
C16 C17 H17 120.8 . . ?
C12 C17 H17 120.8 . . ?
O3 C18 C64 106.8(6) . 3 ?
O3 C18 H18A 110.4 . . ?
C64 C18 H18A 110.4 3 . ?
O3 C18 H18B 110.4 . . ?
C64 C18 H18B 110.4 3 . ?
H18A C18 H18B 108.6 . . ?
O2 C19 C20 107.5(6) . . ?
O2 C19 H19A 110.2 . . ?
C20 C19 H19A 110.2 . . ?
O2 C19 H19B 110.2 . . ?
C20 C19 H19B 110.2 . . ?
H19A C19 H19B 108.5 . . ?
C24 C20 C21 118.4(7) . . ?
C24 C20 C19 122.1(7) . . ?
C21 C20 C19 119.4(7) . . ?
N3 C21 C20 123.4(7) . . ?
N3 C21 H21 118.3 . . ?
C20 C21 H21 118.3 . . ?
N3 C22 C23 122.0(7) . . ?
N3 C22 H22 119.0 . . ?
C23 C22 H22 119.0 . . ?
C22 C23 C24 119.3(7) . . ?
C22 C23 H23 120.4 . . ?
C24 C23 H23 120.4 . . ?
C20 C24 C23 119.2(7) . . ?
C20 C24 H24 120.4 . . ?
C23 C24 H24 120.4 . . ?
N4 C25 C26 124.6(8) . . ?
N4 C25 H25 117.7 . . ?
C26 C25 H25 117.7 . . ?
C25 C26 C27 118.6(8) . . ?
C25 C26 H26 120.7 . . ?
C27 C26 H26 120.7 . . ?
C26 C27 C28 118.5(8) . . ?
C26 C27 H27 120.8 . . ?
C28 C27 H27 120.8 . . ?
C29 C28 C27 118.0(8) . . ?
C29 C28 C54 120.3(7) . 3 ?
C27 C28 C54 121.7(7) . 3 ?
N4 C29 C28 122.6(8) . . ?
N4 C29 H29 118.7 . . ?
C28 C29 H29 118.7 . . ?
C35 C30 C31 119.4(7) . . ?
C35 C30 P2 118.3(7) . . ?
C31 C30 P2 122.3(6) . . ?
C32 C31 C30 120.0(8) . . ?
C32 C31 H31 120.0 . . ?
C30 C31 H31 120.0 . . ?
C33 C32 C31 120.8(9) . . ?
C33 C32 H32 119.6 . . ?
C31 C32 H32 119.6 . . ?
C32 C33 C34 120.2(9) . . ?
C32 C33 H33 119.9 . . ?
C34 C33 H33 119.9 . . ?
C33 C34 C35 119.3(9) . . ?
C33 C34 H34 120.3 . . ?
C35 C34 H34 120.3 . . ?
C30 C35 C34 120.0(9) . . ?
C30 C35 H35 120.0 . . ?
C34 C35 H35 120.0 . . ?
O5 C36 C10 107.7(6) . 3_645 ?
O5 C36 H36A 110.2 . . ?
C10 C36 H36A 110.2 3_645 . ?
O5 C36 H36B 110.2 . . ?
C10 C36 H36B 110.2 3_645 . ?
H36A C36 H36B 108.5 . . ?
O4 C37 C38 106.1(6) . . ?
O4 C37 H37A 110.5 . . ?
C38 C37 H37A 110.5 . . ?
O4 C37 H37B 110.5 . . ?
C38 C37 H37B 110.5 . . ?
H37A C37 H37B 108.7 . . ?
C39 C38 C42 118.3(7) . . ?
C39 C38 C37 120.8(7) . . ?
C42 C38 C37 120.8(7) . . ?
N5 C39 C38 125.0(7) . . ?
N5 C39 H39 117.5 . . ?
C38 C39 H39 117.5 . . ?
N5 C40 C41 124.2(8) . . ?
N5 C40 H40 117.9 . . ?
C41 C40 H40 117.9 . . ?
C42 C41 C40 118.4(8) . . ?
C42 C41 H41 120.8 . . ?
C40 C41 H41 120.8 . . ?
C41 C42 C38 118.6(8) . . ?
C41 C42 H42 120.7 . . ?
C38 C42 H42 120.7 . . ?
N6 C43 C44 122.7(9) . . ?
N6 C43 H43 118.7 . . ?
C44 C43 H43 118.7 . . ?
C43 C44 C45 120.3(9) . . ?
C43 C44 H44 119.9 . . ?
C45 C44 H44 119.9 . . ?
C44 C45 C46 118.7(8) . . ?
C44 C45 H45 120.7 . . ?
C46 C45 H45 120.7 . . ?
C47 C46 C45 117.7(8) . . ?
C47 C46 C72 120.8(8) . 3_455 ?
C45 C46 C72 121.5(8) . 3_455 ?
N6 C47 C46 124.2(8) . . ?
N6 C47 H47 117.9 . . ?
C46 C47 H47 117.9 . . ?
C49 C48 C53 118.4(7) . . ?
C49 C48 P3 125.1(6) . . ?
C53 C48 P3 116.4(6) . . ?
C50 C49 C48 121.1(8) . . ?
C50 C49 H49 119.4 . . ?
C48 C49 H49 119.4 . . ?
C49 C50 C51 120.4(8) . . ?
C49 C50 H50 119.8 . . ?
C51 C50 H50 119.8 . . ?
C52 C51 C50 118.7(8) . . ?
C52 C51 H51 120.7 . . ?
C50 C51 H51 120.7 . . ?
C53 C52 C51 121.4(8) . . ?
C53 C52 H52 119.3 . . ?
C51 C52 H52 119.3 . . ?
C52 C53 C48 119.8(8) . . ?
C52 C53 H53 120.1 . . ?
C48 C53 H53 120.1 . . ?
O7 C54 C28 109.5(6) . 3_545 ?
O7 C54 H54A 109.8 . . ?
C28 C54 H54A 109.8 3_545 . ?
O7 C54 H54B 109.8 . . ?
C28 C54 H54B 109.8 3_545 . ?
H54A C54 H54B 108.2 . . ?
O6 C55 C56 106.6(6) . . ?
O6 C55 H55A 110.4 . . ?
C56 C55 H55A 110.4 . . ?
O6 C55 H55B 110.4 . . ?
C56 C55 H55B 110.4 . . ?
H55A C55 H55B 108.6 . . ?
C60 C56 C57 119.0(7) . . ?
C60 C56 C55 122.0(7) . . ?
C57 C56 C55 118.9(7) . . ?
N7 C57 C56 122.9(7) . . ?
N7 C57 H57 118.6 . . ?
C56 C57 H57 118.6 . . ?
N7 C58 C59 121.9(8) . . ?
N7 C58 H58 119.1 . . ?
C59 C58 H58 119.1 . . ?
C60 C59 C58 118.9(8) . . ?
C60 C59 H59 120.5 . . ?
C58 C59 H59 120.5 . . ?
C56 C60 C59 118.8(8) . . ?
C56 C60 H60 120.6 . . ?
C59 C60 H60 120.6 . . ?
N8 C61 C62 121.8(8) . . ?
N8 C61 H61 119.1 . . ?
C62 C61 H61 119.1 . . ?
C61 C62 C63 119.8(8) . . ?
C61 C62 H62 120.1 . . ?
C63 C62 H62 120.1 . . ?
C62 C63 C64 120.1(7) . . ?
C62 C63 H63 120.0 . . ?
C64 C63 H63 120.0 . . ?
C63 C64 C65 116.9(7) . . ?
C63 C64 C18 124.0(7) . 3_545 ?
C65 C64 C18 119.0(7) . 3_545 ?
N8 C65 C64 123.8(7) . . ?
N8 C65 H65 118.1 . . ?
C64 C65 H65 118.1 . . ?
C71 C66 C67 117.5(7) . . ?
C71 C66 P4 120.6(6) . . ?
C67 C66 P4 121.8(6) . . ?
C66 C67 C68 120.9(9) . . ?
C66 C67 H67 119.6 . . ?
C68 C67 H67 119.6 . . ?
C69 C68 C67 118.0(9) . . ?
C69 C68 H68 121.0 . . ?
C67 C68 H68 121.0 . . ?
C70 C69 C68 122.5(9) . . ?
C70 C69 H69 118.8 . . ?
C68 C69 H69 118.8 . . ?
C69 C70 C71 119.2(9) . . ?
C69 C70 H70 120.4 . . ?
C71 C70 H70 120.4 . . ?
C70 C71 C66 121.7(8) . . ?
C70 C71 H71 119.1 . . ?
C66 C71 H71 119.1 . . ?
O8 C72 C46 108.6(6) . 3_445 ?
O8 C72 H72A 110.0 . . ?
C46 C72 H72A 110.0 3_445 . ?
O8 C72 H72B 110.0 . . ?
C46 C72 H72B 110.0 3_445 . ?
H72A C72 H72B 108.3 . . ?
C74 C73 H73A 109.5 . . ?
C74 C73 H73B 109.5 . . ?
H73A C73 H73B 109.5 . . ?
C74 C73 H73C 109.5 . . ?
H73A C73 H73C 109.5 . . ?
H73B C73 H73C 109.5 . . ?
N9 C74 C73 177.6(18) . . ?
C76 C75 H75A 109.5 . . ?
C76 C75 H75B 109.5 . . ?
H75A C75 H75B 109.5 . . ?
C76 C75 H75C 109.5 . . ?
H75A C75 H75C 109.5 . . ?
H75B C75 H75C 109.5 . . ?
N10 C76 C75 174.3(13) . . ?
C78 C77 H77A 109.5 . . ?
C78 C77 H77B 109.5 . . ?
H77A C77 H77B 109.5 . . ?
C78 C77 H77C 109.5 . . ?
H77A C77 H77C 109.5 . . ?
H77B C77 H77C 109.5 . . ?
N11 C78 C77 177.0(11) . . ?
C80 C79 H79A 109.5 . . ?
C80 C79 H79B 109.5 . . ?
H79A C79 H79B 109.5 . . ?
C80 C79 H79C 109.5 . . ?
H79A C79 H79C 109.5 . . ?
H79B C79 H79C 109.5 . . ?
N12 C80 C79 176.1(11) . . ?
C4 N1 C3 118.3(7) . . ?
C4 N1 Ag1 123.4(5) . . ?
C3 N1 Ag1 118.2(5) . . ?
C7 N2 C11 117.7(7) . . ?
C7 N2 Ag1 122.5(6) . . ?
C11 N2 Ag1 119.1(5) . . ?
C21 N3 C22 117.6(7) . . ?
C21 N3 Ag2 119.7(5) . . ?
C22 N3 Ag2 122.3(5) . . ?
C25 N4 C29 117.7(7) . . ?
C25 N4 Ag2 121.7(6) . . ?
C29 N4 Ag2 120.4(5) . . ?
C40 N5 C39 115.4(7) . . ?
C40 N5 Ag3 126.2(5) . . ?
C39 N5 Ag3 118.2(5) . . ?
C43 N6 C47 116.5(7) . . ?
C43 N6 Ag3 122.2(6) . . ?
C47 N6 Ag3 120.8(5) . . ?
C58 N7 C57 118.3(7) . . ?
C58 N7 Ag4 121.1(5) . . ?
C57 N7 Ag4 120.5(5) . . ?
C65 N8 C61 117.3(7) . . ?
C65 N8 Ag4 117.4(5) . . ?
C61 N8 Ag4 123.5(5) . . ?
C1 O1 P4 119.2(4) . 1_765 ?
C19 O2 P1 116.9(4) . . ?
C18 O3 P1 121.1(4) . . ?
C37 O4 P2 122.1(4) . . ?
C36 O5 P2 120.6(5) . . ?
C55 O6 P3 121.4(4) . . ?
C54 O7 P3 116.5(4) . . ?
C72 O8 P4 118.5(5) . . ?
O3 P1 O2 105.0(3) . . ?
O3 P1 C12 99.7(3) . . ?
O2 P1 C12 98.8(3) . . ?
O3 P1 Ag1 115.19(19) . . ?
O2 P1 Ag1 117.0(2) . . ?
C12 P1 Ag1 118.3(3) . . ?
O4 P2 O5 105.9(3) . . ?
O4 P2 C30 107.2(3) . . ?
O5 P2 C30 98.0(3) . . ?
O4 P2 Ag2 108.6(2) . . ?
O5 P2 Ag2 115.2(2) . . ?
C30 P2 Ag2 120.6(3) . . ?
O6 P3 O7 106.4(3) . . ?
O6 P3 C48 105.5(3) . . ?
O7 P3 C48 98.8(3) . . ?
O6 P3 Ag3 107.92(19) . . ?
O7 P3 Ag3 118.2(2) . . ?
C48 P3 Ag3 118.8(2) . . ?
O8 P4 O1 106.1(3) . 1_345 ?
O8 P4 C66 100.3(3) . . ?
O1 P4 C66 97.2(3) 1_345 . ?
O8 P4 Ag4 116.5(2) . . ?
O1 P4 Ag4 116.3(2) 1_345 . ?
C66 P4 Ag4 117.6(3) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 N1 2.288(6) . ?
Ag1 N2 2.296(6) . ?
Ag1 P1 2.3360(19) . ?
Ag2 N3 2.273(6) . ?
Ag2 N4 2.318(7) . ?
Ag2 P2 2.348(2) . ?
Ag3 N5 2.265(6) . ?
Ag3 N6 2.285(6) . ?
Ag3 P3 2.3623(19) . ?
Ag4 N7 2.270(6) . ?
Ag4 N8 2.296(6) . ?
Ag4 P4 2.352(2) . ?
B1 F2 1.370(11) . ?
B1 F4 1.395(12) . ?
B1 F1 1.400(11) . ?
B1 F3 1.411(11) . ?
B2 F8 1.38(2) . ?
B2 F6 1.399(15) . ?
B2 F5 1.417(15) . ?
B2 F7 1.429(13) . ?
B3 F9 1.366(11) . ?
B3 F12 1.390(11) . ?
B3 F10 1.399(10) . ?
B3 F11 1.410(12) . ?
B4 F15 1.364(15) . ?
B4 F14 1.382(15) . ?
B4 F16 1.396(18) . ?
B4 F13 1.445(16) . ?
C1 O1 1.457(9) . ?
C1 C2 1.522(11) . ?
C1 H1A 0.9900 . ?
C1 H1B 0.9900 . ?
C2 C6 1.379(12) . ?
C2 C3 1.385(10) . ?
C3 N1 1.341(9) . ?
C3 H3 0.9500 . ?
C4 N1 1.339(11) . ?
C4 C5 1.383(12) . ?
C4 H4 0.9500 . ?
C5 C6 1.348(12) . ?
C5 H5 0.9500 . ?
C6 H6 0.9500 . ?
C7 N2 1.305(11) . ?
C7 C8 1.418(12) . ?
C7 H7 0.9500 . ?
C8 C9 1.359(13) . ?
C8 H8 0.9500 . ?
C9 C10 1.407(12) . ?
C9 H9 0.9500 . ?
C10 C11 1.396(11) . ?
C10 C36 1.478(11) 3_655 ?
C11 N2 1.332(10) . ?
C11 H11 0.9500 . ?
C12 C13 1.396(11) . ?
C12 C17 1.399(11) . ?
C12 P1 1.812(8) . ?
C13 C14 1.345(11) . ?
C13 H13 0.9500 . ?
C14 C15 1.451(12) . ?
C14 H14 0.9500 . ?
C15 C16 1.339(12) . ?
C15 H15 0.9500 . ?
C16 C17 1.381(11) . ?
C16 H16 0.9500 . ?
C17 H17 0.9500 . ?
C18 O3 1.468(8) . ?
C18 C64 1.495(10) 3 ?
C18 H18A 0.9900 . ?
C18 H18B 0.9900 . ?
C19 O2 1.456(8) . ?
C19 C20 1.499(10) . ?
C19 H19A 0.9900 . ?
C19 H19B 0.9900 . ?
C20 C24 1.373(11) . ?
C20 C21 1.394(11) . ?
C21 N3 1.344(10) . ?
C21 H21 0.9500 . ?
C22 N3 1.361(10) . ?
C22 C23 1.386(11) . ?
C22 H22 0.9500 . ?
C23 C24 1.394(11) . ?
C23 H23 0.9500 . ?
C24 H24 0.9500 . ?
C25 N4 1.304(10) . ?
C25 C26 1.371(12) . ?
C25 H25 0.9500 . ?
C26 C27 1.378(12) . ?
C26 H26 0.9500 . ?
C27 C28 1.413(12) . ?
C27 H27 0.9500 . ?
C28 C29 1.377(11) . ?
C28 C54 1.505(11) 3 ?
C29 N4 1.359(10) . ?
C29 H29 0.9500 . ?
C30 C35 1.364(12) . ?
C30 C31 1.410(11) . ?
C30 P2 1.814(7) . ?
C31 C32 1.369(12) . ?
C31 H31 0.9500 . ?
C32 C33 1.351(14) . ?
C32 H32 0.9500 . ?
C33 C34 1.397(14) . ?
C33 H33 0.9500 . ?
C34 C35 1.401(13) . ?
C34 H34 0.9500 . ?
C35 H35 0.9500 . ?
C36 O5 1.437(9) . ?
C36 C10 1.478(11) 3_645 ?
C36 H36A 0.9900 . ?
C36 H36B 0.9900 . ?
C37 O4 1.462(8) . ?
C37 C38 1.521(10) . ?
C37 H37A 0.9900 . ?
C37 H37B 0.9900 . ?
C38 C39 1.361(11) . ?
C38 C42 1.395(11) . ?
C39 N5 1.352(10) . ?
C39 H39 0.9500 . ?
C40 N5 1.335(10) . ?
C40 C41 1.395(11) . ?
C40 H40 0.9500 . ?
C41 C42 1.377(12) . ?
C41 H41 0.9500 . ?
C42 H42 0.9500 . ?
C43 N6 1.343(11) . ?
C43 C44 1.357(13) . ?
C43 H43 0.9500 . ?
C44 C45 1.367(14) . ?
C44 H44 0.9500 . ?
C45 C46 1.389(13) . ?
C45 H45 0.9500 . ?
C46 C47 1.365(11) . ?
C46 C72 1.516(12) 3_455 ?
C47 N6 1.352(10) . ?
C47 H47 0.9500 . ?
C48 C49 1.393(11) . ?
C48 C53 1.404(11) . ?
C48 P3 1.807(7) . ?
C49 C50 1.377(11) . ?
C49 H49 0.9500 . ?
C50 C51 1.392(12) . ?
C50 H50 0.9500 . ?
C51 C52 1.386(12) . ?
C51 H51 0.9500 . ?
C52 C53 1.382(11) . ?
C52 H52 0.9500 . ?
C53 H53 0.9500 . ?
C54 O7 1.474(9) . ?
C54 C28 1.505(11) 3_545 ?
C54 H54A 0.9900 . ?
C54 H54B 0.9900 . ?
C55 O6 1.460(8) . ?
C55 C56 1.517(11) . ?
C55 H55A 0.9900 . ?
C55 H55B 0.9900 . ?
C56 C60 1.370(12) . ?
C56 C57 1.396(11) . ?
C57 N7 1.339(10) . ?
C57 H57 0.9500 . ?
C58 N7 1.339(10) . ?
C58 C59 1.407(12) . ?
C58 H58 0.9500 . ?
C59 C60 1.390(12) . ?
C59 H59 0.9500 . ?
C60 H60 0.9500 . ?
C61 N8 1.354(10) . ?
C61 C62 1.366(11) . ?
C61 H61 0.9500 . ?
C62 C63 1.372(11) . ?
C62 H62 0.9500 . ?
C63 C64 1.372(11) . ?
C63 H63 0.9500 . ?
C64 C65 1.395(11) . ?
C64 C18 1.495(10) 3_545 ?
C65 N8 1.342(10) . ?
C65 H65 0.9500 . ?
C66 C71 1.361(12) . ?
C66 C67 1.373(12) . ?
C66 P4 1.821(7) . ?
C67 C68 1.393(13) . ?
C67 H67 0.9500 . ?
C68 C69 1.335(13) . ?
C68 H68 0.9500 . ?
C69 C70 1.333(13) . ?
C69 H69 0.9500 . ?
C70 C71 1.360(12) . ?
C70 H70 0.9500 . ?
C71 H71 0.9500 . ?
C72 O8 1.470(9) . ?
C72 C46 1.516(12) 3_445 ?
C72 H72A 0.9900 . ?
C72 H72B 0.9900 . ?
C73 C74 1.47(2) . ?
C73 H73A 0.9800 . ?
C73 H73B 0.9800 . ?
C73 H73C 0.9800 . ?
C74 N9 1.19(2) . ?
C75 C76 1.453(16) . ?
C75 H75A 0.9800 . ?
C75 H75B 0.9800 . ?
C75 H75C 0.9800 . ?
C76 N10 1.114(13) . ?
C77 C78 1.489(13) . ?
C77 H77A 0.9800 . ?
C77 H77B 0.9800 . ?
C77 H77C 0.9800 . ?
C78 N11 1.116(11) . ?
C79 C80 1.452(13) . ?
C79 H79A 0.9800 . ?
C79 H79B 0.9800 . ?
C79 H79C 0.9800 . ?
C80 N12 1.146(12) . ?
O1 P4 1.610(5) 1_765 ?
O2 P1 1.627(5) . ?
O3 P1 1.602(5) . ?
O4 P2 1.595(6) . ?
O5 P2 1.616(5) . ?
O6 P3 1.603(5) . ?
O7 P3 1.610(6) . ?
O8 P4 1.608(6) . ?
P4 O1 1.610(5) 1_345 ?
