Crystallography Open Database

Information card for entry 4308704

Preview

Coordinates	4308704.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	(21) [Dy(OSiPh3)3(py)3]
Formula	C69 H60 Dy N3 O3 Si3
Calculated formula	C69 Dy N3 O3 Si3
Title of publication	Synthesis and Characterization of a Family of Structurally Characterized Dysprosium Alkoxides for Improved Fatigue-Resistance Characteristics of PDyZT Thin Films
Authors of publication	Timothy J. Boyle; Scott D. Bunge; Paul G. Clem; Jacob Richardson; Jeffrey T. Dawley; Leigh Anna M. Ottley; Mark A. Rodriguez; Bruce A. Tuttle; Gabriel R. Avilucea; Ralph G. Tissot
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	1588 - 1600
a	22.937 ± 0.005 Å
b	22.937 ± 0.005 Å
c	12.123 ± 0.005 Å
α	90°
β	90°
γ	120°
Cell volume	5523 ± 3 Å³
Cell temperature	203 ± 2 K
Ambient diffraction temperature	203 ± 2 K
Number of distinct elements	6
Space group number	160
Hermann-Mauguin space group symbol	R 3 m :H
Hall space group symbol	R 3 -2"
Residual factor for all reflections	0.0644
Residual factor for significantly intense reflections	0.064
Weighted residual factors for significantly intense reflections	0.1619
Weighted residual factors for all reflections included in the refinement	0.1623
Goodness-of-fit parameter for all reflections included in the refinement	1.149
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179125 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/87.	4308704.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4308704.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4308704.cif
5312	2011-01-03	cif/ Adding files, updated with the 'cif_fix_enum' program and the cif_core.dic dictionary. The enumerator values were fixed, mostly incorrect case, but also some values that had extra underscores, dashes or spaces. Unfortunately, 22 had non-ASCII characters with the 8-th bit set, and these got incorrectly interpreted as latin1 characters and converted to their UTF8 equivalents by Perl. To fix the structures, however, they need to be redeposited from the original files with the new CIFParser/cif_filter version.	4308704.cif
1526	2010-09-26	cif/4/ Adding new CIFs from Inorg. Chem. 2005 deposited via Web deposition site to the COD test database (and transferede to the main COD database after renaming).	4308704.cif