Crystallography Open Database

Information card for entry 4309256

Preview

Coordinates	4309256.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H17 Cl N Sb
Calculated formula	C19 H17 Cl N Sb
Title of publication	Synthetic and Structural Studies of Cyclodistib(V)azanes
Authors of publication	May C. Copsey; Sabrina B. Gallon; Sara K. Grocott; John C. Jeffery; Christopher A. Russell; John M. Slattery
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	5495 - 5500
a	11.664 ± 0.002 Å
b	10.549 ± 0.002 Å
c	14.024 ± 0.003 Å
α	90°
β	109.34 ± 0.03°
γ	90°
Cell volume	1628.2 ± 0.6 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0242
Residual factor for significantly intense reflections	0.021
Weighted residual factors for significantly intense reflections	0.0495
Weighted residual factors for all reflections included in the refinement	0.0506
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179130 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/92.	4309256.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4309256.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4309256.cif
1526	2010-09-26	cif/4/ Adding new CIFs from Inorg. Chem. 2005 deposited via Web deposition site to the COD test database (and transferede to the main COD database after renaming).	4309256.cif