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Information card for entry 4309897
Preview
Coordinates | 4309897.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C29 H39 B10 Cl2 N3 Ni |
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Calculated formula | C29 H39 B10 Cl2 N3 Ni |
Title of publication | Synthesis of Nickel-Monocarbollide Complexes by Oxidative Insertion |
Authors of publication | Thomas D. McGrath; Andreas Franken; Jason A. Kautz; F. Gordon A. Stone |
Journal of publication | Inorganic Chemistry |
Year of publication | 2005 |
Journal volume | 44 |
Pages of publication | 8135 - 8144 |
a | 12.558 ± 0.003 Å |
b | 18.357 ± 0.004 Å |
c | 16.282 ± 0.004 Å |
α | 90° |
β | 111.944 ± 0.004° |
γ | 90° |
Cell volume | 3481.5 ± 1.4 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0774 |
Residual factor for significantly intense reflections | 0.0547 |
Weighted residual factors for significantly intense reflections | 0.1559 |
Weighted residual factors for all reflections included in the refinement | 0.1676 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.016 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
179136 (current) | 2016-03-23 | cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/98. |
4309897.cif |
120081 | 2014-07-12 | Adding DOIs to range 4/30 structures. | 4309897.cif |
34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4309897.cif |
31985 | 2012-01-04 | cif/ Canging data item '_diffrn_standards_decay_% none' to '_diffrn_standards_decay_% 0'. |
4309897.cif |
1526 | 2010-09-26 | cif/4/ Adding new CIFs from Inorg. Chem. 2005 deposited via Web deposition site to the COD test database (and transferede to the main COD database after renaming). |
4309897.cif |
All data in the COD and the database itself are dedicated to the
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Users of the data should acknowledge the original authors of the
structural data.