Crystallography Open Database

Information card for entry 4310125

Preview

Coordinates	4310125.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C6 H24 La N6 S4 Sb
Calculated formula	C6 H24 La N6 S4 Sb
Title of publication	Solvothermal Syntheses of [Ln(en)3(H2O)x(μ3-x-SbS4)] (Ln = La,x= 0; Ln = Nd,x= 1) and [Ln(en)4]SbS4.0.5en (Ln = Eu, Dy, Yb): A Systematic Study on the Formation and Crystal Structures of New Lanthanide Thioantimonates(V)
Authors of publication	Dingxian Jia; Qianxin Zhao; Yong Zhang; Jie Dai; Jinglin Zuo
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	8861 - 8867
a	8.723 ± 0.0015 Å
b	10.2043 ± 0.0019 Å
c	20.277 ± 0.004 Å
α	90°
β	93.818 ± 0.005°
γ	90°
Cell volume	1800.9 ± 0.6 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0385
Residual factor for significantly intense reflections	0.0358
Weighted residual factors for significantly intense reflections	0.0577
Weighted residual factors for all reflections included in the refinement	0.0583
Goodness-of-fit parameter for all reflections included in the refinement	1.324
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179140 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/01.	4310125.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4310125.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4310125.cif
1526	2010-09-26	cif/4/ Adding new CIFs from Inorg. Chem. 2005 deposited via Web deposition site to the COD test database (and transferede to the main COD database after renaming).	4310125.cif